Structural and electromagnetic properties of 3D printed and electron beam sintered lithium ferrite ceramic

Bibliographic Details
Parent link:Ceramics International.— .— Amsterdam: Elsevier Science Publishing Company Inc.
Vol. 50, iss. 24, Pt A.— 2024.— P. 52632-52639
Corporate Author: National Research Tomsk Polytechnic University (570)
Other Authors: Lysenko E. N. Elena Nikolaevna, Nikolaev E. V. Evgeny Vladimirovich, Vlasov V. A. Vitaliy Anatolievich, Svirkov Aleksandr Sergeevich A. S., Surzhikov A. P. Anatoly Petrovich, Artishchev S. A. Sergey Aleksandrovich
Summary:Title screen
In this work, the structures and electromagnetic properties of lithium ferrite ceramics manufactured by the additive method, based on the extrusion deposition of ferrite samples with a binder and their subsequent heating with high-energy electron beam, were studied. Preliminary synthesis of ferrite powder was carried out by a solid-phase method using iron oxide and lithium carbonate. To prepare ferrite paste, a binder based on ethylcellulose and terpineol was used. The printed samples were sintered by heating with 1.4 MeV electron beam using an ELV-6 accelerator. Using X-ray phase analysis, it was established that the sintered ceramic consists mainly of an ordered α−Li0.5Fe2.5O4 phase and a certain amount of disordered β−Li0.5Fe2.5O4 phase. Ferrite ceramics are characterized by a relative density of 72.6–92.1 %, specific saturation magnetization of 63–65 emu/g, Curie temperature of 628–630 °C, electrical resistivity of 108–106 Ω cm, depending on the thickness of the printed sample (200 and 400 μm) and sintering temperature (1100 and 1200°С)
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Published: 2024
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Online Access:https://doi.org/10.1016/j.ceramint.2024.10.114
Format: Electronic Book Chapter
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=676876