Benzimidazole-based N-heterocyclic carbene silver complexes as catalysts for the formation of carbonates from carbon dioxide and epoxides; Molecular Catalysis; Vol. 526

Benzimidazole-based N-heterocyclic carbene silver complexes as catalysts for the formation of carbonates from carbon dioxide and epoxides; Molecular Catalysis; Vol. 526

Λεπτομέρειες βιβλιογραφικής εγγραφής
Parent link:	Molecular Catalysis Vol. 526.— 2022.— [112369, 12 p.]
Συγγραφή απο Οργανισμό/Αρχή:	Национальный исследовательский Томский политехнический университет Исследовательская школа химических и биомедицинских технологий
Άλλοι συγγραφείς:	Nawaz Z. Zahid, Ullah H. Habib, Gurbuz N. Nevin, Zafar M. N. Muhammad Naveed, Verpoort F. V. K. Frensis Valter Kornelius, Tahir M. N. Muhammad Nawaz, Ozdemir I. Ismail, Trovitch R. J. Ryan
Περίληψη:	Title screen A series of left-to-right inequivalent 1,3-disubstituted benzimidazolium halide pro-ligands having the general formula [RBNHCCH2OxMe][X] (R = 3-Me-Bn, 3,5-Me2-Bn, 2,4,6-Me3-Bn, 2,3,5,6-Me4-Bn, 2,3,4,5,6-Me5-Bn, 3,4,5-(OMe)3-Bn, or 4-tBu-Bn; X = Cl, Br) were synthesized by the alkylation of 1-((3-methyloxetan-3-yl)methyl)benzimidazole. The corresponding Ag complexes, (RBNHCCH2OxMe)AgX, were prepared following pro-ligand addition to Ag2O. These compounds were characterized using spectroscopic techniques such as FT-IR, NMR spectroscopy, and single-crystal X-ray diffraction. The solid-state structure of (3-Me-BnBNHCCH2OxMe)AgCl revealed a linear monomer while [(2,4,6-Me3-BnBNHCCH2OxMe)AgCl]2 was found to exist as a dimer with pseudo trigonal planar geometry about each metal center. The synthesized (RBNHCCH2OxMe)AgX complexes were found to be efficient for the addition of carbon dioxide to epoxides to yield value-added cyclic carbonates at ambient pressure. Amongst the investigated complexes, the bimetallic complex [(2,4,6-Me3-BnBNHCCH2OxMe)AgCl]2 was found to be the most active for CO2 insertion, exhibiting favorable activity when compared to known NHC complexes. Режим доступа: по договору с организацией-держателем ресурса
Γλώσσα:	Αγγλικά
Έκδοση:	2022
Θέματα:	электронный ресурс труды учёных ТПУ carbon dioxide insertion n-heterocyclic carbene silver complexes cyclic carbonate homogeneous catalysis углекислый газ N-гетероциклические карбены серебро карбонаты гомогенный катализ
Διαθέσιμο Online:	https://doi.org/10.1016/j.mcat.2022.112369
Μορφή:	Ηλεκτρονική πηγή Κεφάλαιο βιβλίου
KOHA link:	https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=668481

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