Transition-Metal-Free Base-Controlled C−N Coupling Reactions: Selective Mono Versus Diarylation of Primary Amines with 2-Chlorobenzimidazoles; Advanced Synthesis and Catalysis; Vol. 363, iss. 5

Dettagli Bibliografici
Parent link:Advanced Synthesis and Catalysis
Vol. 363, iss. 5.— 2021.— [P. 1408-1416]
Ente Autore: Национальный исследовательский Томский политехнический университет Исследовательская школа химических и биомедицинских технологий
Altri autori: Wei Sang, Yan-Yan Gong, Hua Cheng, Rui Zhang, Ye Yuan, Guang-Gao Fan, Zhi-Qin Wang, Cheng Chen, Verpoort F. V. K. Frensis Valter Kornelius
Riassunto:Title screen
Herein, a base-controlled protocol was developed for the C−N coupling of primary amines and 2-chlorobenzimidazoles, affording a handful of secondary or tertiary amines in a selective fashion. Moreover, this protocol was realized under transition-metal-free conditions, and the variation of the base from iPr2NH to LiOtBu completely switched the selectivity from monoarylation to diarylation. Further investigations elucidated that the variety, intrinsic basicity and amount of the utilized bases considerably affected these reactions.
Lingua:inglese
Pubblicazione: 2021
Soggetti:
Accesso online:https://doi.org/10.1002/adsc.202001365
Natura: Elettronico Capitolo di libro
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=667545

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200 1 |a Transition-Metal-Free Base-Controlled C−N Coupling Reactions: Selective Mono Versus Diarylation of Primary Amines with 2-Chlorobenzimidazoles  |f Wei Sang, Yan-Yan Gong, Hua Cheng [et al.] 
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330 |a Herein, a base-controlled protocol was developed for the C−N coupling of primary amines and 2-chlorobenzimidazoles, affording a handful of secondary or tertiary amines in a selective fashion. Moreover, this protocol was realized under transition-metal-free conditions, and the variation of the base from iPr2NH to LiOtBu completely switched the selectivity from monoarylation to diarylation. Further investigations elucidated that the variety, intrinsic basicity and amount of the utilized bases considerably affected these reactions. 
461 |t Advanced Synthesis and Catalysis 
463 |t Vol. 363, iss. 5  |v [P. 1408-1416]  |d 2021 
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610 1 |a diarylation 
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