Effect of processing parameters on in situ screen printing-assisted synthesis and electrical properties of Ti3SiC2-based structures

Bibliographic Details
Parent link:Journal of Advanced Ceramics
Vol. 10, iss. 1.— 2021.— [P. 129-138]
Main Author: Lorenz M. Mylena
Corporate Author: Национальный исследовательский Томский политехнический университет Инженерная школа новых производственных технологий Отделение материаловедения
Other Authors: Travitsky (Travitzky) N. Nakhum, Rambo C. R. Carlos
Summary:Title screen
This work reports on the development of pastes containing Ti, TiC, Si, and C elementary powders for in situ synthesis of Ti3SiC2 via screen printing. Four paste compositions were manufactured using two powder mixtures (Ti/Si/C and Ti/TiC/Si/C) with different stoichiometry. The pastes were screen printed onto Al2O3 substrates and sintered at 1400 °С in argon varying the dwell time from 1 to 5 h. The printed pastes containing TiC and excess of Si exhibited the lowest surface roughness and after 5 h sintering comprised of Ti3SiC2 as the majority phase. The electrical conductivity of this sample was found to range from 4.63•104 to 2.57•105 S·m–1 in a temperature range of 25–400 °С.
Published: 2021
Subjects:
Online Access:https://doi.org/10.1007/s40145-020-0427-0
Format: Electronic Book Chapter
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=665226