Validation of a GC-MS Method for Quantitative Determination of Cyclohexanone by Oxidative Cleavage; Pharmaceutical Chemistry Journal; Vol. 52, iss. 12
| Parent link: | Pharmaceutical Chemistry Journal Vol. 52, iss. 12.— 2019.— [P. 1021-1025] |
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| Altres autors: | , , , , , |
| Sumari: | Title screen A GC method for quantitative determination of cyclohexanone by oxidative cleavage was proposed. The research was aimed at the development of a simple, rapid, and effective GC method for quantitative analysis ofcyclohexanone in a reaction mixture. Chlorobenzene was used as an internal standard. Qualitative analysiscompared mass spectra obtained for each component with mass spectra from the National Institute of Standards and Technology (NIST) database. The method was validated for specificity, linearity, accuracy, robustness, repeatability, and intralaboratory precision. Режим доступа: по договору с организацией-держателем ресурса |
| Idioma: | anglès |
| Publicat: |
2019
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| Matèries: | |
| Accés en línia: | https://doi.org/10.1007/s11094-019-01945-w |
| Format: | MixedMaterials Electrònic Capítol de llibre |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=662817 |
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| 200 | 1 | |a Validation of a GC-MS Method for Quantitative Determination of Cyclohexanone by Oxidative Cleavage |f E. V. Podrezova, M. S. Larkina, M. S. Yusubov [et al.] | |
| 203 | |a Text |c electronic | ||
| 300 | |a Title screen | ||
| 320 | |a [References: 7 tit.] | ||
| 330 | |a A GC method for quantitative determination of cyclohexanone by oxidative cleavage was proposed. The research was aimed at the development of a simple, rapid, and effective GC method for quantitative analysis ofcyclohexanone in a reaction mixture. Chlorobenzene was used as an internal standard. Qualitative analysiscompared mass spectra obtained for each component with mass spectra from the National Institute of Standards and Technology (NIST) database. The method was validated for specificity, linearity, accuracy, robustness, repeatability, and intralaboratory precision. | ||
| 333 | |a Режим доступа: по договору с организацией-держателем ресурса | ||
| 461 | |t Pharmaceutical Chemistry Journal | ||
| 463 | |t Vol. 52, iss. 12 |v [P. 1021-1025] |d 2019 | ||
| 610 | 1 | |a электронный ресурс | |
| 610 | 1 | |a труды учёных ТПУ | |
| 610 | 1 | |a cyclohexanone | |
| 610 | 1 | |a quantitative determination | |
| 610 | 1 | |a oxidative cleavage | |
| 610 | 1 | |a validation | |
| 610 | 1 | |a gas chromatography | |
| 610 | 1 | |a internal standard | |
| 610 | 1 | |a циклогексанон | |
| 610 | 1 | |a количественное определение | |
| 610 | 1 | |a окислительное расщепление | |
| 610 | 1 | |a газовая хроматография | |
| 610 | 1 | |a внутренние стандарты | |
| 701 | 1 | |a Podrezova |b E. V. |c Chemist |c Engineer of Tomsk Polytechnic University |f 1992- |g Ekaterina Vladimirovna |y Tomsk |3 (RuTPU)RU\TPU\pers\40301 |9 21290 | |
| 701 | 1 | |a Larkina |b M. S. |g Mariya Sergeevna |f 1984- |c pharmacist |c Professor; Senior Researcher of the Tomsk Polytechnic University, Doctor of Pharmaceutical Sciences |3 (RuTPU)RU\TPU\pers\46781 |9 22417 | |
| 701 | 1 | |a Yusubov |b M. S. |c chemist |c Professor of Tomsk Polytechnic University, Doctor of chemical sciences |f 1961- |g Mekhman Suleiman-Ogly (Suleimanovich) |3 (RuTPU)RU\TPU\pers\31833 |9 15928 | |
| 701 | 1 | |a Belousov |b M. V. |c chemist |c Professor of Tomsk Polytechnic University, Doctor of Pharmaceutical Sciences |f 1963- |g Mikhail Valerievich |3 (RuTPU)RU\TPU\pers\45418 |9 21924 | |
| 701 | 1 | |a Zamanova |b M. K. |c Chemical Engineer |c engineer of Tomsk Polytechnic University |f 1983- |g Margarita Karimovna |3 (RuTPU)RU\TPU\pers\33834 |9 17423 | |
| 701 | 1 | |a Krivoshchekov |b S. V. |c chemist |c engineer of Tomsk Polytechnic University |f 1987- |g Sergey Vladimirovich |3 (RuTPU)RU\TPU\pers\34574 |9 17936 | |
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