Validation of a GC-MS Method for Quantitative Determination of Cyclohexanone by Oxidative Cleavage

Bibliographische Detailangaben
Parent link:Pharmaceutical Chemistry Journal
Vol. 52, iss. 12.— 2019.— [P. 1021-1025]
Weitere Verfasser: Podrezova E. V. Ekaterina Vladimirovna, Larkina M. S. Mariya Sergeevna, Yusubov M. S. Mekhman Suleiman-Ogly (Suleimanovich), Belousov M. V. Mikhail Valerievich, Zamanova M. K. Margarita Karimovna, Krivoshchekov S. V. Sergey Vladimirovich
Zusammenfassung:Title screen
A GC method for quantitative determination of cyclohexanone by oxidative cleavage was proposed. The research was aimed at the development of a simple, rapid, and effective GC method for quantitative analysis ofcyclohexanone in a reaction mixture. Chlorobenzene was used as an internal standard. Qualitative analysiscompared mass spectra obtained for each component with mass spectra from the National Institute of Standards and Technology (NIST) database. The method was validated for specificity, linearity, accuracy, robustness, repeatability, and intralaboratory precision.
Режим доступа: по договору с организацией-держателем ресурса
Sprache:Englisch
Veröffentlicht: 2019
Schlagworte:
Online-Zugang:https://doi.org/10.1007/s11094-019-01945-w
Format: Elektronisch Buchkapitel
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=662817