Validation of a GC-MS Method for Quantitative Determination of Cyclohexanone by Oxidative Cleavage

Validation of a GC-MS Method for Quantitative Determination of Cyclohexanone by Oxidative Cleavage

Detalles Bibliográficos
Parent link:Pharmaceutical Chemistry Journal
Vol. 52, iss. 12.— 2019.— [P. 1021-1025]
Otros Autores: Podrezova E. V. Ekaterina Vladimirovna, Larkina M. S. Mariya Sergeevna, Yusubov M. S. Mekhman Suleiman-Ogly (Suleimanovich), Belousov M. V. Mikhail Valerievich, Zamanova M. K. Margarita Karimovna, Krivoshchekov S. V. Sergey Vladimirovich
Sumario:Title screen
A GC method for quantitative determination of cyclohexanone by oxidative cleavage was proposed. The research was aimed at the development of a simple, rapid, and effective GC method for quantitative analysis ofcyclohexanone in a reaction mixture. Chlorobenzene was used as an internal standard. Qualitative analysiscompared mass spectra obtained for each component with mass spectra from the National Institute of Standards and Technology (NIST) database. The method was validated for specificity, linearity, accuracy, robustness, repeatability, and intralaboratory precision.
Режим доступа: по договору с организацией-держателем ресурса
Publicado: 2019
Materias:
электронный ресурс
труды учёных ТПУ
cyclohexanone
quantitative determination
oxidative cleavage
validation
gas chromatography
internal standard
циклогексанон
количественное определение
окислительное расщепление
газовая хроматография
внутренние стандарты
Acceso en línea:https://doi.org/10.1007/s11094-019-01945-w
Formato: Electrónico Capítulo de libro
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=662817

Internet

https://doi.org/10.1007/s11094-019-01945-w

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