Validation of a GC-MS Method for Quantitative Determination of Cyclohexanone by Oxidative Cleavage
| Parent link: | Pharmaceutical Chemistry Journal Vol. 52, iss. 12.— 2019.— [P. 1021-1025] |
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| مؤلفون آخرون: | , , , , , |
| الملخص: | Title screen A GC method for quantitative determination of cyclohexanone by oxidative cleavage was proposed. The research was aimed at the development of a simple, rapid, and effective GC method for quantitative analysis ofcyclohexanone in a reaction mixture. Chlorobenzene was used as an internal standard. Qualitative analysiscompared mass spectra obtained for each component with mass spectra from the National Institute of Standards and Technology (NIST) database. The method was validated for specificity, linearity, accuracy, robustness, repeatability, and intralaboratory precision. Режим доступа: по договору с организацией-держателем ресурса |
| منشور في: |
2019
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| الموضوعات: | |
| الوصول للمادة أونلاين: | https://doi.org/10.1007/s11094-019-01945-w |
| التنسيق: | الكتروني فصل الكتاب |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=662817 |
| الملخص: | Title screen A GC method for quantitative determination of cyclohexanone by oxidative cleavage was proposed. The research was aimed at the development of a simple, rapid, and effective GC method for quantitative analysis ofcyclohexanone in a reaction mixture. Chlorobenzene was used as an internal standard. Qualitative analysiscompared mass spectra obtained for each component with mass spectra from the National Institute of Standards and Technology (NIST) database. The method was validated for specificity, linearity, accuracy, robustness, repeatability, and intralaboratory precision. Режим доступа: по договору с организацией-держателем ресурса |
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| DOI: | 10.1007/s11094-019-01945-w |