$Laboratory X-ray Diffraction Complex for In Situ Investigations of Structural Phase Evolution of Materials under Gaseous Atmosphere; Metals; Vol. 10, iss. 4$

Laboratory X-ray Diffraction Complex for In Situ Investigations of Structural Phase Evolution of Materials under Gaseous Atmosphere; Metals; Vol. 10, iss. 4

Бібліографічні деталі
Parent link:	Metals Vol. 10, iss. 4.— 2020.— [447, 15 p.]
Співавтор:	Национальный исследовательский Томский политехнический университет Инженерная школа ядерных технологий Отделение экспериментальной физики
Інші автори:	Syrtanov M. S. Maksim Sergeevich, Garanin G. V. Georgy Viktorovich, Kashkarov E. B. Egor Borisovich, Pushilina N. S. Natalia Sergeevna, Kudiyarov V. N. Victor Nikolaevich, Murashkina T. L. Tatiana Leonidovna
Резюме:	Title screen In this work, a laboratory X-ray diffraction complex for in situ investigations of structural phase evolution of materials under gaseous atmosphere and elevated temperatures was developed. The approbation of the complex was carried out using a commercially pure titanium (CP-Ti) powder, zirconium (Zr-1Nb) alloy and electron beam melted Ti-6Al-4V alloy. It was established that hydrogenation of the CP-Ti powder occurred at a temperature of 500 °C and a hydrogen pressure of 0.5 atm, accompanied by the formation of metastable ? titanium hydride (?-TiH) phase. The lifetime of the ?-TiH phase was 35–40 min. Decomposition of the ?-TiH occurred after reaching a temperature of 650 °C as a result of the thermally stimulated desorption of hydrogen. The a-Zr ? d-ZrH phase transformation was observed under hydrogenation of the zirconium Zr-1Nb alloy at a temperature of 350 °C and a hydrogen pressure of 0.5 atm. It was revealed that the increase in hydrogenation temperature to 450 °C accelerated this transformation by two times. Hydrogenation of the electron beam melted titanium Ti-6Al-4V alloy at a temperature of 650 °C and hydrogen pressure of 0.5 atm was accompanied by the a ? a + Я ? Я + a2 phase transformations.
Мова:	Англійська
Опубліковано:	2020
Предмети:	электронный ресурс труды учёных ТПУ in situ XRD hydrogenation titanium alloys zirconium alloy electron beam melting thermal expansion coefficient рентгенография гидрирование титановые сплавы сплавы циркония электронно-лучевая плавка
Онлайн доступ:	http://earchive.tpu.ru/handle/11683/64876 https://doi.org/10.3390/met10040447
Формат:	MixedMaterials Електронний ресурс Частина з книги
KOHA link:	https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=662171

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