Synthesis and Properties of Nickel/Carbon Nanotube Nanocomposites via the Electrical Explosion of Wire in Liquid and Spark Plasma Sintering Method

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Parent link:Journal of Nanoscience and Nanotechnology
Vol. 17, iss. 10.— 2017.— [P. 7410-7417]
Korporativní autor: Национальный исследовательский Томский политехнический университет Инженерная школа новых производственных технологий Научно-образовательный центр Н. М. Кижнера
Další autoři: Nguyen Minh-Thuyet, Nguyen Hong-Hai, Kim Won Joo, An V. V. Vladimir Vilorievich, Kim Jin Chun
Shrnutí:Title screen
Nickel-carbon nanotube (CNT-Ni) composite powders were successfully synthesized by electrical explosion of Ni wire in an ethanoic-CNT suspension as an ambient condition. The as-prepared CNT-Ni composite powders were then dried, heated at 400 °C in a H2/CO2 environment, completely sintered by using spark plasma sintering at 1100 °C (with a heating rate of 50 °C/min from room temperature) for 10 min under a pressure of 50 MPa in vacuum condition. According to Ranma spectroscopy analysis, the structure of CNTs was not changed after sintering process. A hardness of 3.0 wt.% CNT-Ni composite was improved up to 30.04% compared to pure Ni, but this enhanced hardness was not achieved when the concentrations of CNTs up to 5.0 wt.%, thus setting an empirical reinforcing limit. The main strengthening mechanism for this could be explained by the Hall-Petch effect. The vibrating sample magnetometer analysis results showed that the as-synthesized nickel-carbon nanotube composites were soft ferromagnetic materials.
Режим доступа: по договору с организацией-держателем ресурса
Jazyk:angličtina
Vydáno: 2017
Témata:
On-line přístup:https://doi.org/10.1166/jnn.2017.14777
Médium: Elektronický zdroj Kapitola
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=657897

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330 |a Nickel-carbon nanotube (CNT-Ni) composite powders were successfully synthesized by electrical explosion of Ni wire in an ethanoic-CNT suspension as an ambient condition. The as-prepared CNT-Ni composite powders were then dried, heated at 400 °C in a H2/CO2 environment, completely sintered by using spark plasma sintering at 1100 °C (with a heating rate of 50 °C/min from room temperature) for 10 min under a pressure of 50 MPa in vacuum condition. According to Ranma spectroscopy analysis, the structure of CNTs was not changed after sintering process. A hardness of 3.0 wt.% CNT-Ni composite was improved up to 30.04% compared to pure Ni, but this enhanced hardness was not achieved when the concentrations of CNTs up to 5.0 wt.%, thus setting an empirical reinforcing limit. The main strengthening mechanism for this could be explained by the Hall-Petch effect. The vibrating sample magnetometer analysis results showed that the as-synthesized nickel-carbon nanotube composites were soft ferromagnetic materials. 
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