Synthesis and Properties of Nickel/Carbon Nanotube Nanocomposites via the Electrical Explosion of Wire in Liquid and Spark Plasma Sintering Method
| Parent link: | Journal of Nanoscience and Nanotechnology Vol. 17, iss. 10.— 2017.— [P. 7410-7417] |
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| Other Authors: | , , , , |
| Summary: | Title screen Nickel-carbon nanotube (CNT-Ni) composite powders were successfully synthesized by electrical explosion of Ni wire in an ethanoic-CNT suspension as an ambient condition. The as-prepared CNT-Ni composite powders were then dried, heated at 400 °C in a H2/CO2 environment, completely sintered by using spark plasma sintering at 1100 °C (with a heating rate of 50 °C/min from room temperature) for 10 min under a pressure of 50 MPa in vacuum condition. According to Ranma spectroscopy analysis, the structure of CNTs was not changed after sintering process. A hardness of 3.0 wt.% CNT-Ni composite was improved up to 30.04% compared to pure Ni, but this enhanced hardness was not achieved when the concentrations of CNTs up to 5.0 wt.%, thus setting an empirical reinforcing limit. The main strengthening mechanism for this could be explained by the Hall-Petch effect. The vibrating sample magnetometer analysis results showed that the as-synthesized nickel-carbon nanotube composites were soft ferromagnetic materials. Режим доступа: по договору с организацией-держателем ресурса |
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2017
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| Online Access: | https://doi.org/10.1166/jnn.2017.14777 |
| Format: | Electronic Book Chapter |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=657897 |