4-Iodoantipyrine synthesized by means of solid-state mechanical activation; Pharmaceutical Chemistry Journal; Vol. 41, iss. 3
| Parent link: | Pharmaceutical Chemistry Journal Vol. 41, iss. 3.— 2007.— [P. 154-156] |
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| Other Authors: | , , , |
| Summary: | Title screen Antipyrine and its benzenesulfonate were iodinated by solid-state mechanical activation (in the absence of solvent) under the action of iodine, iodine chloride, Me4N+ICl2-, and Et4N+ICl2- with the formation of 4-iodoantipyrine. The proposed process does not require organic solvents and meets all Green Chemistry demands. The best results were achieved with the use of tetraalkylammonium salts Me4N+ICl2- and Et4N+ICl2-. Режим доступа: по договору с организацией-держателем ресурса |
| Language: | English |
| Published: |
2007
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| Subjects: | |
| Online Access: | http://dx.doi.org/10.1007/s11094-007-0034-1 |
| Format: | xMaterials Electronic Book Chapter |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=654279 |
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| 200 | 1 | |a 4-Iodoantipyrine synthesized by means of solid-state mechanical activation |f E. A . Krasnokutskaya [et al.] | |
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| 300 | |a Title screen | ||
| 320 | |a [References: 11 tit.] | ||
| 330 | |a Antipyrine and its benzenesulfonate were iodinated by solid-state mechanical activation (in the absence of solvent) under the action of iodine, iodine chloride, Me4N+ICl2-, and Et4N+ICl2- with the formation of 4-iodoantipyrine. The proposed process does not require organic solvents and meets all Green Chemistry demands. The best results were achieved with the use of tetraalkylammonium salts Me4N+ICl2- and Et4N+ICl2-. | ||
| 333 | |a Режим доступа: по договору с организацией-держателем ресурса | ||
| 461 | |t Pharmaceutical Chemistry Journal | ||
| 463 | |t Vol. 41, iss. 3 |v [P. 154-156] |d 2007 | ||
| 610 | 1 | |a электронный ресурс | |
| 610 | 1 | |a труды учёных ТПУ | |
| 610 | 1 | |a синтез | |
| 610 | 1 | |a активация | |
| 610 | 1 | |a антипирин | |
| 610 | 1 | |a иодирование | |
| 610 | 1 | |a тетраалкиламмониевые соли | |
| 610 | 1 | |a зеленая химия | |
| 701 | 1 | |a Krasnokutskaya |b E. A . |c organic chemist |c Professor of Tomsk Polytechnic University, Doctor of chemical sciences |f 1966- |g Elena Aleksandrovna |3 (RuTPU)RU\TPU\pers\31829 |9 15924 | |
| 701 | 1 | |a Trusova |b M. E. |c organic chemist |c Associate professor of Tomsk Polytechnic University, Candidate of chemical sciences |f 1982- |g Marina Evgenievna |3 (RuTPU)RU\TPU\pers\31823 |9 15918 | |
| 701 | 1 | |a Gibert |b N. S. | |
| 701 | 1 | |a Filimonov |b V. D. |c Russian chemist |c Professor of the TPU |f 1945- |g Viktor Dmitrievich |3 (RuTPU)RU\TPU\pers\26423 |9 12127 | |
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