4-Iodoantipyrine synthesized by means of solid-state mechanical activation

Bibliographic Details
Parent link:Pharmaceutical Chemistry Journal
Vol. 41, iss. 3.— 2007.— [P. 154-156]
Other Authors: Krasnokutskaya E. A . Elena Aleksandrovna, Trusova M. E. Marina Evgenievna, Gibert N. S., Filimonov V. D. Viktor Dmitrievich
Summary:Title screen
Antipyrine and its benzenesulfonate were iodinated by solid-state mechanical activation (in the absence of solvent) under the action of iodine, iodine chloride, Me4N+ICl2-, and Et4N+ICl2- with the formation of 4-iodoantipyrine. The proposed process does not require organic solvents and meets all Green Chemistry demands. The best results were achieved with the use of tetraalkylammonium salts Me4N+ICl2- and Et4N+ICl2-.
Режим доступа: по договору с организацией-держателем ресурса
Language:English
Published: 2007
Subjects:
Online Access:http://dx.doi.org/10.1007/s11094-007-0034-1
Format: Electronic Book Chapter
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=654279