4-Iodoantipyrine synthesized by means of solid-state mechanical activation

Bibliographische Detailangaben
Parent link:	Pharmaceutical Chemistry Journal Vol. 41, iss. 3.— 2007.— [P. 154-156]
Weitere Verfasser:	Krasnokutskaya E. A . Elena Aleksandrovna, Trusova M. E. Marina Evgenievna, Gibert N. S., Filimonov V. D. Viktor Dmitrievich
Zusammenfassung:	Title screen Antipyrine and its benzenesulfonate were iodinated by solid-state mechanical activation (in the absence of solvent) under the action of iodine, iodine chloride, Me4N+ICl2-, and Et4N+ICl2- with the formation of 4-iodoantipyrine. The proposed process does not require organic solvents and meets all Green Chemistry demands. The best results were achieved with the use of tetraalkylammonium salts Me4N+ICl2- and Et4N+ICl2-. Режим доступа: по договору с организацией-держателем ресурса
Sprache:	Englisch
Veröffentlicht:	2007
Schlagworte:	электронный ресурс труды учёных ТПУ синтез активация антипирин иодирование тетраалкиламмониевые соли зеленая химия
Online-Zugang:	http://dx.doi.org/10.1007/s11094-007-0034-1
Format:	Elektronisch Buchkapitel
KOHA link:	https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=654279

Beschreibung
Zusammenfassung:	Title screen Antipyrine and its benzenesulfonate were iodinated by solid-state mechanical activation (in the absence of solvent) under the action of iodine, iodine chloride, Me4N+ICl2-, and Et4N+ICl2- with the formation of 4-iodoantipyrine. The proposed process does not require organic solvents and meets all Green Chemistry demands. The best results were achieved with the use of tetraalkylammonium salts Me4N+ICl2- and Et4N+ICl2-. Режим доступа: по договору с организацией-держателем ресурса
DOI:	10.1007/s11094-007-0034-1

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