Analytical control of lactide synthesis; Petroleum and Coal; Vol. 58, iss. 5

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Parent link:Petroleum and Coal
Vol. 58, iss. 5.— 2016.— [P. 567-572]
Korporativní autor: Национальный исследовательский Томский политехнический университет (ТПУ) Институт природных ресурсов (ИПР) Кафедра технологии органических веществ и полимерных материалов (ТОВПМ)
Další autoři: Krutas D. S. Darjya Sergeevna, Zamanova M. K. Margarita Karimovna, Lukjyanov A. E. Aleksandr Evgenjevich, Zinovyev (Zinovjev, Zinoviev) A. L. Alexey Leonidovich, Novikov V. T. Viktor Timofeevich, Volgina T. N. Tatiana Nikolaevna
Shrnutí:Title screen
The technique of identification and quantification of D,L-lactide, lactic acid and its oligomers by the method of high performance liquid chromatography (HPLC) was developed. The separation was done on two columns connected consecutively using an aqueous solution of orthophosphoric acid and acetonitrile in the ratio 88:12 vol. % at a flow rate of 1.2 ml min-1 as a mobile phase. The developed method is simple and linear. Research of specificity, accuracy, repeatability and reproducibility shows that the technique is suitable for analytical control of all stages of the lactide synthesis from lactic acid.
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Jazyk:angličtina
Vydáno: 2016
Témata:
On-line přístup:http://www.vurup.sk/wp-content/uploads/dlm_uploads/2017/07/pc_6_2016_krutas_volgina_488cor.pdf
Médium: Elektronický zdroj Kapitola
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=653525