Analytical control of lactide synthesis

Detaylı Bibliyografya
Parent link:Petroleum and Coal
Vol. 58, iss. 5.— 2016.— [P. 567-572]
Müşterek Yazar: Национальный исследовательский Томский политехнический университет (ТПУ) Институт природных ресурсов (ИПР) Кафедра технологии органических веществ и полимерных материалов (ТОВПМ)
Diğer Yazarlar: Krutas D. S. Darjya Sergeevna, Zamanova M. K. Margarita Karimovna, Lukjyanov A. E. Aleksandr Evgenjevich, Zinovyev (Zinovjev, Zinoviev) A. L. Alexey Leonidovich, Novikov V. T. Viktor Timofeevich, Volgina T. N. Tatiana Nikolaevna
Özet:Title screen
The technique of identification and quantification of D,L-lactide, lactic acid and its oligomers by the method of high performance liquid chromatography (HPLC) was developed. The separation was done on two columns connected consecutively using an aqueous solution of orthophosphoric acid and acetonitrile in the ratio 88:12 vol. % at a flow rate of 1.2 ml min-1 as a mobile phase. The developed method is simple and linear. Research of specificity, accuracy, repeatability and reproducibility shows that the technique is suitable for analytical control of all stages of the lactide synthesis from lactic acid.
Свободный доступ из сети Интернет
Dil:İngilizce
Baskı/Yayın Bilgisi: 2016
Konular:
Online Erişim:http://www.vurup.sk/wp-content/uploads/dlm_uploads/2017/07/pc_6_2016_krutas_volgina_488cor.pdf
Materyal Türü: Elektronik Kitap Bölümü
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=653525