Preparation and X-ray Structural Study of 1-Arylbenziodoxolones; The Journal of Organic Chemistry; Vol. 78, iss. 8
| Parent link: | The Journal of Organic Chemistry.— , 1936- Vol. 78, iss. 8.— 2013.— [P. 3767-3773] |
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| Korporativní autor: | |
| Další autoři: | , , , |
| Shrnutí: | Title screen Various 1-arylbenziodoxolones can be conveniently prepared from 2-iodobenzoic acid and arenes by a one-pot procedure using Oxone (2KHSO5·KHSO4·K2SO4) as an inexpensive and environmentally safe oxidant. This procedure is also applicable for the synthesis of the 7-methylbenziodoxolone ring system using 2-iodo-3-methylbenzoic acid as starting compound. Structures of four 1-arylbenziodoxolone derivatives were established by single-crystal X-ray diffraction analysis. An enhanced reactivity of 1-aryl-7-methylbenziodoxolones toward nucleophiles compared to unsubstituted 1-arylbenziodoxolones has been found. Режим доступа: по договору с организацией-держателем ресурса |
| Jazyk: | angličtina |
| Vydáno: |
2013
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| Témata: | |
| On-line přístup: | http://dx.doi.org/10.1021/jo400212u |
| Médium: | MixedMaterials Elektronický zdroj Kapitola |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=650158 |
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| 200 | 1 | |a Preparation and X-ray Structural Study of 1-Arylbenziodoxolones |f M. S. Yusubov [et al.] | |
| 203 | |a Text |c electronic | ||
| 300 | |a Title screen | ||
| 320 | |a [References: p. 3773 (15 tit.)] | ||
| 330 | |a Various 1-arylbenziodoxolones can be conveniently prepared from 2-iodobenzoic acid and arenes by a one-pot procedure using Oxone (2KHSO5·KHSO4·K2SO4) as an inexpensive and environmentally safe oxidant. This procedure is also applicable for the synthesis of the 7-methylbenziodoxolone ring system using 2-iodo-3-methylbenzoic acid as starting compound. Structures of four 1-arylbenziodoxolone derivatives were established by single-crystal X-ray diffraction analysis. An enhanced reactivity of 1-aryl-7-methylbenziodoxolones toward nucleophiles compared to unsubstituted 1-arylbenziodoxolones has been found. | ||
| 333 | |a Режим доступа: по договору с организацией-держателем ресурса | ||
| 461 | |t The Journal of Organic Chemistry |d 1936- | ||
| 463 | |t Vol. 78, iss. 8 |v [P. 3767-3773] |d 2013 | ||
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