Kinetic Analysis of Lithium-Zinc Ferrite Synthesis by Thermogravimetric Method

Bibliographic Details
Parent link:Advanced Materials Research: Scientific Journal
Vol. 1085 : Prospects of Fundamental Sciences Development (PFSD-2014).— 2015.— [P. 255-259]
Main Author: Nikolaev E. V. Evgeny Vladimirovich
Corporate Authors: Национальный исследовательский Томский политехнический университет (ТПУ) Институт неразрушающего контроля (ИНК) Проблемная научно-исследовательская лаборатория электроники, диэлектриков и полупроводников (ПНИЛ ЭДиП), Национальный исследовательский Томский политехнический университет (ТПУ) Институт неразрушающего контроля (ИНК) Кафедра физических методов и приборов контроля качества (ФМПК)
Other Authors: Surzhikov A. P. Anatoly Petrovich, Lysenko E. N. Elena Nikolaevna
Summary:Title screen
The kinetic of lithium-zinc ferrite synthesis reaction up to temperatures 800°С was studied in air using non-isothermal thermogravimetric analysis. Mathematical treatment of thermogravimetric curves was carried out using Netzsch Thermokinetics software where the kinetic model with minimal adjustable parameters quantitatively describe the synthesis reaction of lithium-zinc ferrite was chosen. It was shown that the experimental TG curves clearly suggest a multi-step process for the ferrite synthesis and therefore a model-fitting kinetic analysis based on multivariate non-linear regressions was conducted. The complex reaction can be best described with a three-step reaction scheme consisting of parallel reaction steps. It is established that the best results were obtained with the using at the first stage the diffusion model of Yander, on the second and third stage were used the reactions of n-order. Kinetic parameters of lithium-zinc ferrite synthesis reaction were found.
Режим доступа: по договору с организацией-держателем ресурса
Published: 2015
Series:Structure Materials, Mechanics and Dynamics of Materials
Subjects:
Online Access:http://dx.doi.org/10.4028/www.scientific.net/AMR.1085.255
Format: Electronic Book Chapter
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=641212