High-Temperature Oxidation of Laminated Ta/Ti3Al(Si)C2 Composites in the Temperature Range 800–1300°C; Journal of Surface Investigation. X-ray, Synchrotron and Neutron Techniques; Vol. 19, iss. 5
| Parent link: | Journal of Surface Investigation. X-ray, Synchrotron and Neutron Techniques.— .— Road Town: Pleiades Publishing, Ltd. Vol. 19, iss. 5.— 2025.— P. 1231–1238 |
|---|---|
| Other Authors: | Kashkarov E. B. Egor Borisovich, Pushilina N. S. Natalia Sergeevna, Abdulmenova A. V. Anastasiya Vladimirovna, Sedanova E. P. Elizaveta Pavlovna, Gusev K. S. Kirill Sergeevich, Syrtanov M. S. Maksim Sergeevich |
| Summary: | Title screen The paper presents the results of a study of high-temperature oxidation in air of the metal-ceramic layered Ti3Al(Si)C2/Ta composites. The composites were made of preceramic papers filled with Ti3Al(Si)C2 and metal foils (Ta) by spark plasma sintering. The sintering temperature was 1250°C, the holding time was 5 min, and the pressure was 50 MPa. The corrosion resistance of the laminated Ti3Al(Si)C2/Ta composites was estimated based on the results of high-temperature oxidation in air. The phase composition and microstructure of the oxide layers were analyzed by X-ray diffraction and scanning electron microscopy, respectively. It has been found that the Ti3Al(Si)C2/Ta composites demonstrate high oxidation resistance in the temperature range 800–1200°C due to the formation of a dense Al2O3 layer on the outer surface of Ti3Al(Si)C2. With an increase in the oxidation temperature to 1300°C, a complex oxide layer is formed, consisting of an outer TiO2/SiO2/Al2TiO5 layer and an inner TiO2/Al2O3 oxide layer. The thickness of the TiO2/Al2O3 oxide layers formed on the surface of the Ti3Al(Si)C2/Ta composite at oxidation temperatures up to 900°C is less than 1 μm, at a temperature of 1200°C the thickness of the oxide layers is 3.5 μm, and at 1300°C it is 56 μm Текстовый файл AM_Agreement |
| Language: | English |
| Published: |
2025
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| Subjects: | |
| Online Access: | https://doi.org/10.1134/S1027451025701769 |
| Format: | Electronic Book Chapter |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=687390 |
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