Ti3SiC2-based composites synthesized by vacuum sintering and consolidated by spark plasma sintering: Microstructure and mechanical properties; Ceramics International; Vol. 52, iss. 15, Pt. B

Ti3SiC2-based composites synthesized by vacuum sintering and consolidated by spark plasma sintering: Microstructure and mechanical properties; Ceramics International; Vol. 52, iss. 15, Pt. B

Bibliografiske detaljer
Parent link:	Ceramics International.— .— Amsterdam: Elsevier Science Publishing Company Inc. Vol. 52, iss. 15, Pt. B.— 2026.— P. 30302-30314
Andre forfattere:	Sedanova E. P. Elizaveta Pavlovna, Arlashkin I. E. Iljya Evgenjevich, Perevislov S. N. Sergey Nikolaevich, Kashkarov E. B. Egor Borisovich, Pirozhkov A. V. Alexey Vladimirovich, Nassyrbayev (Nasyrbaev) A. Artur, Chemerevskaya K. O. Kseniya Olegovna
Summary:	Title screen The study demonstrates that using pre-synthesized Ti3SiC2 as a precursor is an effective strategy for fabricating high-performance MAX-phase composites. Initial porous Ti3SiC2-TiC composites were obtained by vacuum sintering of 3Ti/1.2Si/2C, Ti/1.2Si/2TiC, 2Ti/1.2SiC/1.8TiC, and 3Ti/1.2SiC/0.8C powder mixtures, and then consolidated by spark plasma sintering (SPS) with reactive Si additions. This two-step approach promoted in-situ Ti3SiC2 formation during SPS, resulting in dense Ti3SiC2-TiSi2-TiC composites with a high MAX-phase content (up to 87 vol%) and a flexural strength of 573–719 MPa – approximately 1.5 times higher than that of composites produced by direct one-step SPS. In contrast, the one-step SPS approach, while effective for producing hard Ti3SiC2-TiC-SiC composite (16.6 GPa), could not achieve comparable strength due to inherent porosity and limited MAX-phase content Текстовый файл AM_Agreement
Sprog:	engelsk
Udgivet:	2026
Fag:	Ceramic composites MAX-Phases Ti3SiC2 Spark plasma sintering Vacuum sintering Mechanical properties электронный ресурс труды учёных ТПУ
Online adgang:	https://doi.org/10.1016/j.ceramint.2026.05.130
Format:	Electronisk Book Chapter
KOHA link:	https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=686762

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