In Situ High-Temperature Synchrotron X-ray Studies of Microstructure and Phase Composition of Additively Fabricated Ti–6Al–4V/TiC Metal Matrix Composite; Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques; Vol. 19, iss. 4

Bibliographic Details
Parent link:Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques.— .— New York: Springer Science+Business Media LLC.
Vol. 19, iss. 4.— 2025.— P. 980-988
Other Authors: Panin A. V. Alexey Viktorovich, Syrtanov M. S. Maksim Sergeevich, Lobova T. A. Tatjyana Anatoljevna, Perevalova O. B. Olga Borisovna, Kazachenok M. S. Marina Sergeevna
Summary:The microstructure and phase composition of Ti–6Al–4V/TiC metal matrix composite samples obtained by wire-feed electron-beam additive manufacturing are investigated by X-ray diffraction analysis and optical, scanning, and transmission electron microscopy. It is shown that the microstructure of the Ti–6Al–4V/TiC composite consists of primary β-grains containing α/α′-plates separated by interlayers of residual β- and α′′-phases. Irregularly shaped TiC carbide particles with sizes of 1–2 µm are distributed along the boundaries of the primary β-grains. The changes in the phase composition of the 3D-printed Ti–6Al–4V/TiC composites during heating from room temperature to 1100°C are investigated by X-ray diffraction using synchrotron radiation. The changes in the shape and position of the X-ray peaks of α/α′- and β-phases during heating and cooling are analyzed. It is shown that in the temperature range of 700–800°C, there is a shift of the 110 peak of the β-phase towards large angles, as well as a change in its full width at half maximum associated with the formation and subsequent decomposition of the orthorhombic α′′-phase
Текстовый файл
AM_Agreement
Language:English
Published: 2025
Subjects:
Online Access:https://doi.org/10.1134/S102745102570140X
Format: Electronic Book Chapter
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=683588

MARC

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330 |a The microstructure and phase composition of Ti–6Al–4V/TiC metal matrix composite samples obtained by wire-feed electron-beam additive manufacturing are investigated by X-ray diffraction analysis and optical, scanning, and transmission electron microscopy. It is shown that the microstructure of the Ti–6Al–4V/TiC composite consists of primary β-grains containing α/α′-plates separated by interlayers of residual β- and α′′-phases. Irregularly shaped TiC carbide particles with sizes of 1–2 µm are distributed along the boundaries of the primary β-grains. The changes in the phase composition of the 3D-printed Ti–6Al–4V/TiC composites during heating from room temperature to 1100°C are investigated by X-ray diffraction using synchrotron radiation. The changes in the shape and position of the X-ray peaks of α/α′- and β-phases during heating and cooling are analyzed. It is shown that in the temperature range of 700–800°C, there is a shift of the 110 peak of the β-phase towards large angles, as well as a change in its full width at half maximum associated with the formation and subsequent decomposition of the orthorhombic α′′-phase 
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461 1 |t Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques  |c New York  |n Springer Science+Business Media LLC. 
463 1 |t Vol. 19, iss. 4  |v P. 980-988  |d 2025 
610 1 |a additive manufacturing 
610 1 |a titanium metal matrix composite 
610 1 |a Ti–6Al–4V/TiC 
610 1 |a microstructure 
610 1 |a phase composition 
610 1 |a in situ high-temperature synchrotron studies 
610 1 |a transmission electron microscopy 
610 1 |a электронный ресурс 
610 1 |a труды учёных ТПУ 
701 1 |a Panin  |b A. V.  |c physicist  |c Professor of Tomsk Polytechnic University, doctor of physical and mathematical Sciences  |f 1971-  |g Alexey Viktorovich  |9 17992 
701 1 |a Syrtanov  |b M. S.  |c physicist  |c Associate Professor, Researcher of Tomsk Polytechnic University, Candidate of Technical Sciences  |f 1990-  |g Maksim Sergeevich  |9 18114 
701 1 |a Lobova  |b T. A.  |g Tatjyana Anatoljevna 
701 1 |a Perevalova  |b O. B.  |g Olga Borisovna 
701 1 |a Kazachenok  |b M. S.  |g Marina Sergeevna 
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