Strategic Synthesis and Supramolecular Organization of Arylenebis(aryliodonium) Salts; Journal of Organic Chemistry; Vol. 90, iss.44

Strategic Synthesis and Supramolecular Organization of Arylenebis(aryliodonium) Salts; Journal of Organic Chemistry; Vol. 90, iss.44

التفاصيل البيبلوغرافية
Parent link:	Journal of Organic Chemistry.— .— Washington: American Chemical Society Vol. 90, iss.44.— 2025.— P. 15542-15554
مؤلفون آخرون:	Knyazeva E. V. Elizaveta Vyacheslavovna, Soldatova N. S. Nataliya Sergeevna, Abramov P. A. Pavel Aleksandrovich, Ivanov D. M. Daniil Mikhaylovich, Burykina Ju. V. Julia, Radzhabov A. D. Amirbek Dzhurabekovich, Yusubov M. S. Mekhman Suleiman-Ogly (Suleimanovich), Resnati D. P. Dzhuzeppe Paolo, Kukushkin V. Yu. Vadim Yurjevich, Postnikov P. S. Pavel Sergeevich
الملخص:	Title screen A comprehensive synthetic toolkit was developed for the preparation of arylenebis(aryliodonium) salts from diiodoarenes via m-CPBA oxidation. The methodology offers versatile approaches that can be adapted based on the solubility of reaction intermediates, enabling either one-pot or two-stage synthesis pathways. Four distinct synthetic methods were established, accommodating a wide range of arenes and diiodoarenes, including sterically hindered and electron-deficient substrates. The resulting bis(iodonium) salts were isolated in good to excellent yields (up to 99%). X-ray crystallographic analysis of these compounds revealed intriguing supramolecular organization in the solid state, with the formation of 1D chains through halogen bonding interactions. These self-assembled architectures demonstrate the potential of bis(iodonium) cations as valuable building blocks for applications in crystal engineering Текстовый файл
اللغة:	الإنجليزية
منشور في:	2025
الموضوعات:	электронный ресурс труды учёных ТПУ
الوصول للمادة أونلاين:	https://doi.org/10.1021/acs.joc.5c01508
التنسيق:	الكتروني فصل الكتاب
KOHA link:	https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=683111

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