$Refinement of Unit Cell Parameters on Modern Single-Crystal Diffractometers. Study of the Anisotropy of the α-33S Single Crystal Thermal Expansion; Crystallography Reports; Vol. 69, iss. 4$

Refinement of Unit Cell Parameters on Modern Single-Crystal Diffractometers. Study of the Anisotropy of the α-33S Single Crystal Thermal Expansion; Crystallography Reports; Vol. 69, iss. 4

Chi tiết về thư mục
Parent link:	Crystallography Reports=Кристаллография.— .— New York: Pleiades Publishing, Inc. Vol. 69, iss. 4.— 2024.— P. 513-521
Tác giả của công ty:	Томский политехнический университет (570)
Tác giả khác:	Serebrennikova P. S. Polina Sergeevna, Panchenko A. V., Egorov N. B. Nikolai Borisovich, Gromilov S. A. Sergey Aleksandrovich
Tóm tắt:	Title screen A technique for refining unit cell parameters of crystals belonging to arbitrary systems on modern single-crystal diffractometers is described. The technique is based on the 2D-detector position calibration. The elementary orthorhombic unit cell parameters of the α-33S single crystal have been refined. The anisotropy of change in the parameters in the range of 90–350 K has been analyzed. The relative increase in the parameter c is shown to be 6.4%. The obtained dependences are approximated by second–third degree polynomials. The absolute and relative increments in the unit cell volume were found to be 138.4 Å3 and 4.3%, respectively. The temperature dependences of the thermal-expansion tensor elements have been refined. The coefficients of thermal expansion of α-33S at room temperature turned out to be α11 = 15.35 × 10–5, α22 = 8.56 × 10–5, and α33 = 9.12 × 10–5 K–1 Текстовый файл AM_Agreement
Ngôn ngữ:	Tiếng Anh
Được phát hành:	2024
Những chủ đề:	труды учёных ТПУ электронный ресурс
Truy cập trực tuyến:	https://doi.org/10.1134/S1063774524601412 Статья на русском языке
Định dạng:	Điện tử Chương của sách
KOHA link:	https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=676805

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