Formation of Ag-Fe Bimetallic Nano-Species on Mordenite Depending on the Initial Ratio of Components; Materials; Vol. 16, iss. 8

Bibliographic Details
Parent link:Materials
Vol. 16, iss. 8.— 2023.— [3026, 17 p.]
Corporate Author: Национальный исследовательский Томский политехнический университет Исследовательская школа химических и биомедицинских технологий
Other Authors: Kotolevich Yu. Yulia, Khramov E. Evgeny, Sanchez-Lopez P. Perla, Pestryakov A. N. Aleksey Nikolaevich, Zubavichus Ya. Yan, Antunez-Garcia J. Joel, Petranovskii V. Vitalii
Summary:Title screen
The formation and properties of silver and iron nanoscale components in the Ag-Fe bimetallic system deposited on mordenite depend on several parameters during their preparation. Previously, it was shown that an important condition for optimizing nano-center properties in a bimetallic catalyst is to change the order of sequential deposition of components; the order “first Ag+, then Fe2+” was chosen as optimal. In this work, the influence of exact Ag/Fe atomic proportion on the system’s physicochemical properties was studied. This ratio has been confirmed to affect the stoichiometry of the reduction–oxidation processes involving Ag+ and Fe2+, as shown by XRD, DR UV-Vis, XPS, and XAFS data, while HRTEM, SBET and TPD-NH3 show little change. However, it was found the correlation between the occurrence and amount of the Fe3+ ions incorporated into the zeolite’s framework and the experimentally determined catalytic activities towards the model de-NOx reaction along the series of nanomaterials elucidated in this present paper.
Language:English
Published: 2023
Subjects:
Online Access:https://doi.org/10.3390/ma16083026
Format: Electronic Book Chapter
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=669456

MARC

LEADER 00000naa0a2200000 4500
001 669456
005 20250211105407.0
035 |a (RuTPU)RU\TPU\network\40696 
035 |a RU\TPU\network\40622 
090 |a 669456 
100 |a 20230516d2023 k||y0rusy50 ba 
101 0 |a eng 
102 |a CH 
135 |a drcn ---uucaa 
181 0 |a i  
182 0 |a b 
200 1 |a Formation of Ag-Fe Bimetallic Nano-Species on Mordenite Depending on the Initial Ratio of Components  |f Yu. Kotolevich, E. Khramov, P. Sanchez-Lopez [et al.] 
203 |a Text  |c electronic 
300 |a Title screen 
320 |a [References: 58 tit.] 
330 |a The formation and properties of silver and iron nanoscale components in the Ag-Fe bimetallic system deposited on mordenite depend on several parameters during their preparation. Previously, it was shown that an important condition for optimizing nano-center properties in a bimetallic catalyst is to change the order of sequential deposition of components; the order “first Ag+, then Fe2+” was chosen as optimal. In this work, the influence of exact Ag/Fe atomic proportion on the system’s physicochemical properties was studied. This ratio has been confirmed to affect the stoichiometry of the reduction–oxidation processes involving Ag+ and Fe2+, as shown by XRD, DR UV-Vis, XPS, and XAFS data, while HRTEM, SBET and TPD-NH3 show little change. However, it was found the correlation between the occurrence and amount of the Fe3+ ions incorporated into the zeolite’s framework and the experimentally determined catalytic activities towards the model de-NOx reaction along the series of nanomaterials elucidated in this present paper. 
461 |t Materials 
463 |t Vol. 16, iss. 8  |v [3026, 17 p.]  |d 2023 
610 1 |a электронный ресурс 
610 1 |a труды учёных ТПУ 
610 1 |a mordenite 
610 1 |a silver 
610 1 |a iron 
610 1 |a ion exchange 
610 1 |a Ag/Fe ratio 
610 1 |a мордениты 
610 1 |a серебро 
610 1 |a железо 
610 1 |a ионный обмен 
701 1 |a Kotolevich  |b Yu.  |g Yulia 
701 1 |a Khramov  |b E.  |g Evgeny 
701 1 |a Sanchez-Lopez  |b P.  |g Perla 
701 1 |a Pestryakov  |b A. N.  |c Chemist  |c Professor of Tomsk Polytechnic University, Doctor of Chemical Science  |f 1963-  |g Aleksey Nikolaevich  |3 (RuTPU)RU\TPU\pers\30471  |9 14796 
701 1 |a Zubavichus  |b Ya.  |g Yan 
701 1 |a Antunez-Garcia  |b J.  |g Joel 
701 1 |a Petranovskii  |b V.  |g Vitalii 
712 0 2 |a Национальный исследовательский Томский политехнический университет  |b Исследовательская школа химических и биомедицинских технологий  |c (2017- )  |3 (RuTPU)RU\TPU\col\23537 
801 2 |a RU  |b 63413507  |c 20230516  |g RCR 
856 4 |u https://doi.org/10.3390/ma16083026 
942 |c CF