Spark plasma sintering of Nb/Ti3Al(Si)C2-TiC laminated composites

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Parent link:Materialia
Vol. 27.— 2023.— [101673, 6 p.]
Korporace: Национальный исследовательский Томский политехнический университет Инженерная школа энергетики Отделение электроэнергетики и электротехники, Национальный исследовательский Томский политехнический университет Инженерная школа ядерных технологий Отделение экспериментальной физики
Další autoři: Kashkarov E. B. Egor Borisovich, Krotkevich D. G. Dmitry Georgievich, Abdulmenova A. V. Anastasiya Vladimirovna, Ivashutenko A. S. Alexander Sergeevich, Perevislov S. N. Sergey Nikolaevich, Lider A. M. Andrey Markovich, Travitsky (Travitzky) N. Nakhum
Shrnutí:Title screen
This work describes novel Nb/Ti3Al(Si)C2-TiC laminated composites fabricated by spark plasma sintering (SPS) at 1250 °C, 50 MPa for 5 min. Preceramic papers filled with Ti3Al(Si)C2 MAX-phase and Nb foils were used as feedstock. Microstructure, phase composition and mechanical properties were evaluated by scanning electron microscopy, X-ray diffraction and three-point bending test, respectively. It was found that the reaction of preceramic paper-derived layers with Nb layers results in the formation of 16.5 µm-thick interlayers mainly composed of columnar Nb-Al intermetallic, Ti-Nb-Si and Nb-Si based phases. The laminated composites showed a brittle-ductile fracture behavior characterized by multiple deflection and branching of cracks at interfaces and plastic deformation of Nb layers. Crack deflection and delamination occur mainly near the interface between the reaction layer and ceramic layer due to the presence of more brittle silicide and carbide phases. The flexural strength of the fabricated composites was ~350 MPa at 1.5% strain.
Режим доступа: по договору с организацией-держателем ресурса
Vydáno: 2023
Témata:
On-line přístup:https://doi.org/10.1016/j.mtla.2023.101673
Médium: Elektronický zdroj Kapitola
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=669176

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