Spark plasma sintering of Nb/Ti3Al(Si)C2-TiC laminated composites; Materialia; Vol. 27

Detalles Bibliográficos
Parent link:Materialia
Vol. 27.— 2023.— [101673, 6 p.]
Corporate Authors: Национальный исследовательский Томский политехнический университет Инженерная школа энергетики Отделение электроэнергетики и электротехники, Национальный исследовательский Томский политехнический университет Инженерная школа ядерных технологий Отделение экспериментальной физики
Outros autores: Kashkarov E. B. Egor Borisovich, Krotkevich D. G. Dmitry Georgievich, Abdulmenova A. V. Anastasiya Vladimirovna, Ivashutenko A. S. Alexander Sergeevich, Perevislov S. N. Sergey Nikolaevich, Lider A. M. Andrey Markovich, Travitsky (Travitzky) N. Nakhum
Summary:Title screen
This work describes novel Nb/Ti3Al(Si)C2-TiC laminated composites fabricated by spark plasma sintering (SPS) at 1250 °C, 50 MPa for 5 min. Preceramic papers filled with Ti3Al(Si)C2 MAX-phase and Nb foils were used as feedstock. Microstructure, phase composition and mechanical properties were evaluated by scanning electron microscopy, X-ray diffraction and three-point bending test, respectively. It was found that the reaction of preceramic paper-derived layers with Nb layers results in the formation of 16.5 µm-thick interlayers mainly composed of columnar Nb-Al intermetallic, Ti-Nb-Si and Nb-Si based phases. The laminated composites showed a brittle-ductile fracture behavior characterized by multiple deflection and branching of cracks at interfaces and plastic deformation of Nb layers. Crack deflection and delamination occur mainly near the interface between the reaction layer and ceramic layer due to the presence of more brittle silicide and carbide phases. The flexural strength of the fabricated composites was ~350 MPa at 1.5% strain.
Режим доступа: по договору с организацией-держателем ресурса
Idioma:inglés
Publicado: 2023
Subjects:
Acceso en liña:https://doi.org/10.1016/j.mtla.2023.101673
Formato: Electrónico Capítulo de libro
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=669176

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200 1 |a Spark plasma sintering of Nb/Ti3Al(Si)C2-TiC laminated composites  |f E. B. Kashkarov, D. G. Krotkevich, A. V. Abdulmenova [et al.] 
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330 |a This work describes novel Nb/Ti3Al(Si)C2-TiC laminated composites fabricated by spark plasma sintering (SPS) at 1250 °C, 50 MPa for 5 min. Preceramic papers filled with Ti3Al(Si)C2 MAX-phase and Nb foils were used as feedstock. Microstructure, phase composition and mechanical properties were evaluated by scanning electron microscopy, X-ray diffraction and three-point bending test, respectively. It was found that the reaction of preceramic paper-derived layers with Nb layers results in the formation of 16.5 µm-thick interlayers mainly composed of columnar Nb-Al intermetallic, Ti-Nb-Si and Nb-Si based phases. The laminated composites showed a brittle-ductile fracture behavior characterized by multiple deflection and branching of cracks at interfaces and plastic deformation of Nb layers. Crack deflection and delamination occur mainly near the interface between the reaction layer and ceramic layer due to the presence of more brittle silicide and carbide phases. The flexural strength of the fabricated composites was ~350 MPa at 1.5% strain. 
333 |a Режим доступа: по договору с организацией-держателем ресурса 
461 |t Materialia 
463 |t Vol. 27  |v [101673, 6 p.]  |d 2023 
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610 1 |a труды учёных ТПУ 
610 1 |a preceramic paper 
610 1 |a laminated composites 
610 1 |a spark plasma sintering 
610 1 |a MAX phases 
610 1 |a microstructure 
610 1 |a прекерамические бумаги 
610 1 |a ламинированные композиты 
701 1 |a Kashkarov  |b E. B.  |c Physicist  |c Associate Professor, Researcher of Tomsk Polytechnic University, Candidate of Physical and Mathematical Sciences  |f 1991-  |g Egor Borisovich  |3 (RuTPU)RU\TPU\pers\34949  |9 18267 
701 1 |a Krotkevich  |b D. G.  |c physicist  |c engineer of Tomsk Polytechnic University  |f 1990-  |g Dmitry Georgievich  |3 (RuTPU)RU\TPU\pers\46798 
701 1 |a Abdulmenova  |b A. V.  |c physicist  |c engineer at Tomsk Polytechnic University  |f 2001-  |g Anastasiya Vladimirovna  |9 88516 
701 1 |a Ivashutenko  |b A. S.  |c specialist in the field of electrical engineering  |c Associate Professor of the Tomsk Polytechnic University, Candidate of technical sciences  |f 1981-  |g Alexander Sergeevich  |3 (RuTPU)RU\TPU\pers\33076  |9 16908 
701 1 |a Perevislov  |b S. N.  |g Sergey Nikolaevich 
701 1 |a Lider  |b A. M.  |c Physicist  |c Professor of Tomsk Polytechnic University, Doctor of Technical Sciences  |f 1976-2025  |g Andrey Markovich  |y Tomsk  |3 (RuTPU)RU\TPU\pers\30400  |9 14743 
701 1 |a Travitsky (Travitzky)  |b N.  |c specialist in the field of material science  |c Professor of Tomsk Polytechnic University  |f 1951-  |g Nakhum  |3 (RuTPU)RU\TPU\pers\42461 
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