A Laser Reduced Graphene Oxide Grid Electrode for the Voltammetric Determination of Carbaryl; Molecules; Vol. 26, iss. 16

Xehetasun bibliografikoak
Parent link:Molecules
Vol. 26, iss. 16.— 2021.— [5050, 12 p.]
Erakunde egilea: Национальный исследовательский Томский политехнический университет Инженерная школа природных ресурсов Отделение химической инженерии
Beste egile batzuk: Saqib M. Muhammad, Dorozhko E. V. Elena Vladimirovna, Barek J. Jiri, Vyskocil V. Vlastimil, Korotkova E. I. Elena Ivanovna, Shabalina A. V. Anastasiya Valerjevna
Gaia:Title screen
Laser-reduced graphene oxide (LRGO) on a polyethylene terephthalate (PET) substrate was prepared in one step to obtain the LRGO grid electrode for sensitive carbaryl determination. The grid form results in a grid distribution of different electrochemically active zones affecting the electroactive substance diffusion towards the electrode surface and increasing the electrochemical sensitivity for carbaryl determination. Carbaryl is electrochemically irreversibly oxidized at the secondary amine moiety of the molecule with the loss of one proton and one electron in the pH range from 5 to 7 by linear scan voltammetry (LSV) on the LRGO grid electrode with a scan rate of 300 mV/s. Some interference of the juice matrix molecules does not significantly affect the LSV oxidation current of carbaryl on the LRGO grid electrode after adsorptive accumulation without applied potential. The LRGO grid electrode can be used for LSV determination of carbaryl in fruit juices in the concentration range from 0.25 to 128 mg/L with LOD of 0.1 mg/L. The fabrication of the LRGO grid electrode opens up possibilities for further inexpensive monitoring of carbaryl in other fruit juices and fruits.
Hizkuntza:ingelesa
Argitaratua: 2021
Gaiak:
Sarrera elektronikoa:http://earchive.tpu.ru/handle/11683/70717
https://doi.org/10.3390/molecules26165050
Formatua: Baliabide elektronikoa Liburu kapitulua
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=667741

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200 1 |a A Laser Reduced Graphene Oxide Grid Electrode for the Voltammetric Determination of Carbaryl  |f M. Saqib, E. V. Dorozhko, J. Barek [et al.] 
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330 |a Laser-reduced graphene oxide (LRGO) on a polyethylene terephthalate (PET) substrate was prepared in one step to obtain the LRGO grid electrode for sensitive carbaryl determination. The grid form results in a grid distribution of different electrochemically active zones affecting the electroactive substance diffusion towards the electrode surface and increasing the electrochemical sensitivity for carbaryl determination. Carbaryl is electrochemically irreversibly oxidized at the secondary amine moiety of the molecule with the loss of one proton and one electron in the pH range from 5 to 7 by linear scan voltammetry (LSV) on the LRGO grid electrode with a scan rate of 300 mV/s. Some interference of the juice matrix molecules does not significantly affect the LSV oxidation current of carbaryl on the LRGO grid electrode after adsorptive accumulation without applied potential. The LRGO grid electrode can be used for LSV determination of carbaryl in fruit juices in the concentration range from 0.25 to 128 mg/L with LOD of 0.1 mg/L. The fabrication of the LRGO grid electrode opens up possibilities for further inexpensive monitoring of carbaryl in other fruit juices and fruits. 
461 |t Molecules 
463 |t Vol. 26, iss. 16  |v [5050, 12 p.]  |d 2021 
610 1 |a труды учёных ТПУ 
610 1 |a электронный ресурс 
610 1 |a laser reduced graphene oxide 
610 1 |a grid electrode 
610 1 |a graphene oxide 
610 1 |a linear sweep voltammetry 
610 1 |a carbaryl 
610 1 |a pesticides 
610 1 |a оксид графена 
610 1 |a вольтамперометрия 
610 1 |a карбарил 
610 1 |a пестициды 
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701 1 |a Dorozhko  |b E. V.  |c chemist  |c Engineer of Tomsk Polytechnic University  |f 1979-  |g Elena Vladimirovna  |3 (RuTPU)RU\TPU\pers\32174  |9 16175 
701 1 |a Barek  |b J.  |c Czech chemist  |c Professor of Tomsk Polytechnic University, candidate of chemical Sciences  |f 1949-  |g Jiri  |3 (RuTPU)RU\TPU\pers\39743 
701 1 |a Vyskocil  |b V.  |g Vlastimil 
701 1 |a Korotkova  |b E. I.  |c chemist  |c Professor of Tomsk Polytechnic University, Doctor of chemical science  |f 1965-  |g Elena Ivanovna  |3 (RuTPU)RU\TPU\pers\31278  |9 15456 
701 1 |a Shabalina  |b A. V.  |g Anastasiya Valerjevna 
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