Functionally graded laminated composites fabricated from MAX-phase filled preceramic papers: Microstructure, mechanical properties and oxidation resistance; Journal of the European Ceramic Society; Vol. 42, iss. 5
| Parent link: | Journal of the European Ceramic Society Vol. 42, iss. 5.— 2022.— [P. 2062-2072] |
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| Autores Corporativos: | , |
| Otros Autores: | , , , , , , |
| Sumario: | Title screen This paper describes the fabrication and characterization of novel preceramic paper-derived functionally graded materials (FGMs) based on Ti3(Si,Al)C2 MAX phase. The FGMs with different architecture were fabricated via spark plasma sintering of stacked preceramic papers at 1250 °C for 5 min. Microstructure, phase composition and elemental distribution were analyzed by scanning electron microscopy, X-ray diffraction and energy-dispersive X-ray spectroscopy, respectively. Oxidation tests were performed in air at 1300 °C for 5 h. FGMs containing Al- and Si-enriched MAX-phase layers were formed. The fabricated materials exhibit high flexural strength (over 600 MPa), which are dependent on microstructure and composition of individual layers as well as the architecture of composites. It was found that texturing of MAX phase grains during SPS results in anisotropic hardness of the composite. The difference in the composition of the individual layers also provides a hardness gradient in the composite. It was shown that the formation of the outer layer from the Al-enriched Ti3Al(Si)C2 MAX phase increases the corrosion resistance of Ti3SiC2-based composites. The high corrosion resistance of FGMs is due to the growth of a continuous and dense Al2O3 oxide layer. Режим доступа: по договору с организацией-держателем ресурса |
| Lenguaje: | inglés |
| Publicado: |
2022
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| Materias: | |
| Acceso en línea: | https://doi.org/10.1016/j.jeurceramsoc.2022.01.023 |
| Formato: | Electrónico Capítulo de libro |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=666896 |
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| 200 | 1 | |a Functionally graded laminated composites fabricated from MAX-phase filled preceramic papers: Microstructure, mechanical properties and oxidation resistance |f E. B. Kashkarov, D. G. Krotkevich, Yu. R. Mingazova [et al.] | |
| 203 | |a Text |c electronic | ||
| 300 | |a Title screen | ||
| 320 | |a [References: 73 tit.] | ||
| 330 | |a This paper describes the fabrication and characterization of novel preceramic paper-derived functionally graded materials (FGMs) based on Ti3(Si,Al)C2 MAX phase. The FGMs with different architecture were fabricated via spark plasma sintering of stacked preceramic papers at 1250 °C for 5 min. Microstructure, phase composition and elemental distribution were analyzed by scanning electron microscopy, X-ray diffraction and energy-dispersive X-ray spectroscopy, respectively. Oxidation tests were performed in air at 1300 °C for 5 h. FGMs containing Al- and Si-enriched MAX-phase layers were formed. The fabricated materials exhibit high flexural strength (over 600 MPa), which are dependent on microstructure and composition of individual layers as well as the architecture of composites. It was found that texturing of MAX phase grains during SPS results in anisotropic hardness of the composite. The difference in the composition of the individual layers also provides a hardness gradient in the composite. It was shown that the formation of the outer layer from the Al-enriched Ti3Al(Si)C2 MAX phase increases the corrosion resistance of Ti3SiC2-based composites. The high corrosion resistance of FGMs is due to the growth of a continuous and dense Al2O3 oxide layer. | ||
| 333 | |a Режим доступа: по договору с организацией-держателем ресурса | ||
| 338 | |b Российский научный фонд |d 19-19-00192 | ||
| 461 | |t Journal of the European Ceramic Society | ||
| 463 | |t Vol. 42, iss. 5 |v [P. 2062-2072] |d 2022 | ||
| 610 | 1 | |a электронный ресурс | |
| 610 | 1 | |a труды учёных ТПУ | |
| 610 | 1 | |a preceramic paper | |
| 610 | 1 | |a max-phases | |
| 610 | 1 | |a functionally graded materials | |
| 610 | 1 | |a laminated composites | |
| 610 | 1 | |a spark plasma sintering | |
| 610 | 1 | |a прекерамические бумаги | |
| 610 | 1 | |a искровое плазменное спекание | |
| 610 | 1 | |a многослойные композиты | |
| 610 | 1 | |a микроструктуры | |
| 610 | 1 | |a механические свойства | |
| 610 | 1 | |a стойкость | |
| 610 | 1 | |a окисление | |
| 701 | 1 | |a Kashkarov |b E. B. |c Physicist |c Associate Professor, Researcher of Tomsk Polytechnic University, Candidate of Physical and Mathematical Sciences |f 1991- |g Egor Borisovich |3 (RuTPU)RU\TPU\pers\34949 |9 18267 | |
| 701 | 1 | |a Krotkevich |b D. G. |c physicist |c engineer of Tomsk Polytechnic University |f 1990- |g Dmitry Georgievich |3 (RuTPU)RU\TPU\pers\46798 | |
| 701 | 1 | |a Mingazova |b Yu. R. |c Specialist in the field of nuclear technologies |c Engineer of Tomsk Polytechnic University |f 1998- |g Yuliya Rafailovna |3 (RuTPU)RU\TPU\pers\47088 | |
| 701 | 1 | |a Pushilina |b N. S. |c physicist |c associate Professor of Tomsk Polytechnic University, candidate of physico-mathematical Sciences |f 1984- |g Natalia Sergeevna |3 (RuTPU)RU\TPU\pers\30838 |9 15085 | |
| 701 | 1 | |a Syrtanov |b M. S. |c physicist |c Associate Professor, Researcher of Tomsk Polytechnic University, Candidate of Technical Sciences |f 1990- |g Maksim Sergeevich |3 (RuTPU)RU\TPU\pers\34764 |9 18114 | |
| 701 | 1 | |a Lider |b A. M. |c Physicist |c Professor of Tomsk Polytechnic University, Doctor of Technical Sciences |f 1976-2025 |g Andrey Markovich |y Tomsk |3 (RuTPU)RU\TPU\pers\30400 |9 14743 | |
| 701 | 1 | |a Travitsky (Travitzky) |b N. |c specialist in the field of material science |c Professor of Tomsk Polytechnic University |f 1951- |g Nakhum |3 (RuTPU)RU\TPU\pers\42461 | |
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| 712 | 0 | 2 | |a Национальный исследовательский Томский политехнический университет |b Инженерная школа новых производственных технологий |b Отделение материаловедения |3 (RuTPU)RU\TPU\col\23508 |
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