Glow Discharge Optical Emission Spectrometer Calibration Using Hydrogenated Zr-2.5Nb Alloy Standard Samples

Glow Discharge Optical Emission Spectrometer Calibration Using Hydrogenated Zr-2.5Nb Alloy Standard Samples

書誌詳細
Parent link:	Metals Vol. 8, iss. 5.— 2018.— [372, 9 p.]
団体著者:	Национальный исследовательский Томский политехнический университет Инженерная школа ядерных технологий Отделение экспериментальной физики
その他の著者:	Pryamushko T. S. Tatjyana Sergeevna, Mikhaylov (Mikhailov) A. A. Andrey Anatolievich, Babikhina M. N. Maria, Kudiyarov V. N. Victor Nikolaevich, Laptev R. S. Roman Sergeevich
要約:	Title screen Currently, standard samples of hydrogen-metal systems meeting the requirements of glow discharge optical emission spectrometers (GD-OES) are not available on the market. This article describes the preparation of Zr-Nb-H standard samples and the calibration of GD-OES with the usage of these samples. Samples of Zr-2.5Nb were chosen as the material for sample production. The creation procedure includes five main steps: sample preparation (polishing to an average roughness, Ra, of 0.04 m using sandpaper), annealing, hydrogenation, maintenance in an inert gas atmosphere, and characterization of the samples. The absolute hydrogen concentration in the samples was determined volumetrically and calculated from the weight change. The distribution of hydrogen was studied using GD-OES Profiler 2 by Jobin Yvon Emission Horiba Group. As a result of this work, calibration curves of Zr, H, Nb, O, and other elements were obtained. The calibration errors were in the range of 1-5%.
言語:	英語
出版事項:	2018
主題:	электронный ресурс труды учёных ТПУ GD-OES hydrogen standard samples zirconium alloy водород стандартные образцы циркониевые сплавы тлеющие разряды калибровка спектрометры
オンライン･アクセス:	https://doi.org/10.3390/met8050372
フォーマット:	電子媒体図書の章
KOHA link:	https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=666522

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