Glow Discharge Optical Emission Spectrometer Calibration Using Hydrogenated Zr-2.5Nb Alloy Standard Samples; Metals; Vol. 8, iss. 5
| Parent link: | Metals Vol. 8, iss. 5.— 2018.— [372, 9 p.] |
|---|---|
| Corporate Author: | |
| Other Authors: | , , , , |
| Summary: | Title screen Currently, standard samples of hydrogen-metal systems meeting the requirements of glow discharge optical emission spectrometers (GD-OES) are not available on the market. This article describes the preparation of Zr-Nb-H standard samples and the calibration of GD-OES with the usage of these samples. Samples of Zr-2.5Nb were chosen as the material for sample production. The creation procedure includes five main steps: sample preparation (polishing to an average roughness, Ra, of 0.04 m using sandpaper), annealing, hydrogenation, maintenance in an inert gas atmosphere, and characterization of the samples. The absolute hydrogen concentration in the samples was determined volumetrically and calculated from the weight change. The distribution of hydrogen was studied using GD-OES Profiler 2 by Jobin Yvon Emission Horiba Group. As a result of this work, calibration curves of Zr, H, Nb, O, and other elements were obtained. The calibration errors were in the range of 1-5%. |
| Language: | English |
| Published: |
2018
|
| Subjects: | |
| Online Access: | https://doi.org/10.3390/met8050372 |
| Format: | Electronic Book Chapter |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=666522 |
MARC
| LEADER | 00000naa0a2200000 4500 | ||
|---|---|---|---|
| 001 | 666522 | ||
| 005 | 20251122071715.0 | ||
| 035 | |a (RuTPU)RU\TPU\network\37726 | ||
| 035 | |a RU\TPU\network\29082 | ||
| 090 | |a 666522 | ||
| 100 | |a 20211228d2018 k||y0rusy50 ba | ||
| 101 | 0 | |a eng | |
| 102 | |a CH | ||
| 135 | |a drcn ---uucaa | ||
| 181 | 0 | |a i | |
| 182 | 0 | |a b | |
| 200 | 1 | |a Glow Discharge Optical Emission Spectrometer Calibration Using Hydrogenated Zr-2.5Nb Alloy Standard Samples |f T. S. Pryamushko, A. A. Mikhaylov (Mikhailov), M. N. Babikhina [et al.] | |
| 203 | |a Text |c electronic | ||
| 300 | |a Title screen | ||
| 320 | |a [References: 33 tit.] | ||
| 330 | |a Currently, standard samples of hydrogen-metal systems meeting the requirements of glow discharge optical emission spectrometers (GD-OES) are not available on the market. This article describes the preparation of Zr-Nb-H standard samples and the calibration of GD-OES with the usage of these samples. Samples of Zr-2.5Nb were chosen as the material for sample production. The creation procedure includes five main steps: sample preparation (polishing to an average roughness, Ra, of 0.04 m using sandpaper), annealing, hydrogenation, maintenance in an inert gas atmosphere, and characterization of the samples. The absolute hydrogen concentration in the samples was determined volumetrically and calculated from the weight change. The distribution of hydrogen was studied using GD-OES Profiler 2 by Jobin Yvon Emission Horiba Group. As a result of this work, calibration curves of Zr, H, Nb, O, and other elements were obtained. The calibration errors were in the range of 1-5%. | ||
| 461 | |t Metals | ||
| 463 | |t Vol. 8, iss. 5 |v [372, 9 p.] |d 2018 | ||
| 610 | 1 | |a электронный ресурс | |
| 610 | 1 | |a труды учёных ТПУ | |
| 610 | 1 | |a GD-OES | |
| 610 | 1 | |a hydrogen | |
| 610 | 1 | |a standard samples | |
| 610 | 1 | |a zirconium alloy | |
| 610 | 1 | |a водород | |
| 610 | 1 | |a стандартные образцы | |
| 610 | 1 | |a циркониевые сплавы | |
| 610 | 1 | |a тлеющие разряды | |
| 610 | 1 | |a калибровка | |
| 610 | 1 | |a спектрометры | |
| 701 | 1 | |a Pryamushko |b T. S. |g Tatjyana Sergeevna | |
| 701 | 1 | |a Mikhaylov (Mikhailov) |b A. A. |c Physicist |c Engineer of the Department of Tomsk Polytechnic University |f 1994- |g Andrey Anatolievich |3 (RuTPU)RU\TPU\pers\37483 | |
| 701 | 1 | |a Babikhina |b M. N. |g Maria | |
| 701 | 1 | |a Kudiyarov |b V. N. |c physicist |c Associate Professor of Tomsk Polytechnic University, Candidate of Technical Sciences |f 1990- |g Victor Nikolaevich |y Tomsk |3 (RuTPU)RU\TPU\pers\30836 |9 15083 | |
| 701 | 1 | |a Laptev |b R. S. |c physicist, specialist in the field of non-destructive testing |c Associate Professor of Tomsk Polytechnic University, Doctor of Technical Sciences |f 1987- |g Roman Sergeevich |y Tomsk |3 (RuTPU)RU\TPU\pers\31884 |9 15956 | |
| 712 | 0 | 2 | |a Национальный исследовательский Томский политехнический университет |b Инженерная школа ядерных технологий |b Отделение экспериментальной физики |3 (RuTPU)RU\TPU\col\23549 |
| 801 | 2 | |a RU |b 63413507 |c 20211228 |g RCR | |
| 856 | 4 | |u https://doi.org/10.3390/met8050372 | |
| 942 | |c CF | ||