Determination of Platinum and Rhodium by Stripping Voltammetry; Journal of Analytical Chemistry; Vol. 76, iss. 12

Determination of Platinum and Rhodium by Stripping Voltammetry; Journal of Analytical Chemistry; Vol. 76, iss. 12

Bibliografiske detaljer
Parent link:	Journal of Analytical Chemistry Vol. 76, iss. 12.— 2021.— [P. 1433–1435]
Hovedforfatter:	Egoshina A. V. Anastasiya Vladimirovna
Institution som forfatter:	Национальный исследовательский Томский политехнический университет Инженерная школа природных ресурсов Отделение химической инженерии
Andre forfattere:	Kolpakova N. A. Nina Alexandrovna
Summary:	Title screen We studied the determination of platinum(IV) and rhodium(III) without separating them in solution by stripping voltammetry using the peak of the selective electrooxidation of lead from a lead–platinum–rhodium electrolytic deposit at a potential of –0.3 V. Lead, platinum, and rhodium were electrodeposited in situ on a graphite electrode surface from 1 M HCl. In an electrolytic deposit, platinum and rhodium did not form solid solutions but formed intermetallic compounds (IMCs) with lead. The selective electrooxidation of lead from the PtPb IMC and rhodium from the Pb2Rh IMC occurred at –0.3 V. Platinum(IV) and rhodium(III) can be determined without separation using the standard addition method. The lower limit of determination for platinum(IV) by the peak of the selective electrooxidation of lead from the PbPt IMC is 0.86 mg/L. The lower limit of determination for rhodium(III) by the peak of the selective electrooxidation of lead from the Pb2Rh IMC is 0.0046 mg/L. Режим доступа: по договору с организацией-держателем ресурса
Sprog:	engelsk
Udgivet:	2021
Fag:	труды учёных ТПУ электронный ресурс graphite electrodes electrolytic lead–platinum–rhodium deposit stripping voltammetry графитовые электроды электролитические осадки зачистная вольтамперометрия
Online adgang:	https://doi.org/10.1134/S1061934821120054
Format:	Electronisk Book Chapter
KOHA link:	https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=666481

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