Effect of the Beam Current during the Electron-Beam Melting of Titanium Alloy Ti-6Al-4V on the Structural Features and Phase Transitions in Gas-Phase Hydrogenation

Bibliographic Details
Parent link:Journal of Surface Investigation. X-ray, Synchrotron and Neutron Techniques
Vol. 13, No. 3.— 2019.— [P. 429-433]
Corporate Authors: Национальный исследовательский Томский политехнический университет Инженерная школа ядерных технологий Отделение экспериментальной физики, Национальный исследовательский Томский политехнический университет Институт неразрушающего контроля Международная научно-образовательная лаборатория неразрушающего контроля
Other Authors: Pushilina N. S. Natalia Sergeevna, Kudiyarov V. N. Victor Nikolaevich, Syrtanov M. S. Maksim Sergeevich, Kashkarov E. B. Egor Borisovich
Summary:Title screen
The structure of the titanium alloy Ti-6Al-4V manufactured by electron-beam melting is shown to be represented by initial [beta]-phase grains more than 40 [mu]m in size; the internal volume of the grains is filled with [alpha]-phase precipitates in the form of plates. The average size of the [alpha] plates is 1.6, 2, and 5 [mu]m at beam currents of 2, 2.5, and 3 mA, respectively. In situ X-ray diffractometry using synchrotron radiation shows that the phase transitions in the titanium alloy are divided into three main stages during hydrogenation to a concentration of 0.6 wt % at a temperature of 650°C and a pressure of 1 atm. An increase in the beam current from 2 to 3 mA does not significantly affect the phase composition of the alloy. During hydrogenation, the growth rate of the volume concentration of the [beta] phase is lower at a higher beam current. This indicates a decrease in the rate of hydrogen absorption with increasing beam current, which is associated with an increase in the size of [alpha] plates.
Режим доступа: по договору с организацией-держателем ресурса
Published: 2019
Subjects:
Online Access:https://doi.org/10.1134/S1027451019030170
Format: Electronic Book Chapter
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=664366
Description
Summary:Title screen
The structure of the titanium alloy Ti-6Al-4V manufactured by electron-beam melting is shown to be represented by initial [beta]-phase grains more than 40 [mu]m in size; the internal volume of the grains is filled with [alpha]-phase precipitates in the form of plates. The average size of the [alpha] plates is 1.6, 2, and 5 [mu]m at beam currents of 2, 2.5, and 3 mA, respectively. In situ X-ray diffractometry using synchrotron radiation shows that the phase transitions in the titanium alloy are divided into three main stages during hydrogenation to a concentration of 0.6 wt % at a temperature of 650°C and a pressure of 1 atm. An increase in the beam current from 2 to 3 mA does not significantly affect the phase composition of the alloy. During hydrogenation, the growth rate of the volume concentration of the [beta] phase is lower at a higher beam current. This indicates a decrease in the rate of hydrogen absorption with increasing beam current, which is associated with an increase in the size of [alpha] plates.
Режим доступа: по договору с организацией-держателем ресурса
DOI:10.1134/S1027451019030170