Ferromagnetically Coupled S=1 Chains in Crystals of Verdazyl-Nitronyl Nitroxide Diradicals; Angewandte Chemie International Edition; Vol. 59, iss. 46

Dettagli Bibliografici
Parent link:Angewandte Chemie International Edition
Vol. 59, iss. 46.— 2020.— [P. 20704-20710]
Ente Autore: Национальный исследовательский Томский политехнический университет Исследовательская школа химических и биомедицинских технологий
Altri autori: Tretjyakov E. V. Evgeny Viktorovich, Zhivetjeva S. I. Svetlana Ivanovna, Petunin P. V. Pavel Vasilievich, Gorbunov D. E. Dmitry Evgenjevich, Gritsan N. P. Nina Petrovna, Bagryanskaya I. Yu. Irina Yurjevna, Bogomyakov A. S. Artem Stepanovich, Postnikov P. S. Pavel Sergeevich, Kazantsev M. S. Maksim Sergeevich, Trusova M. E. Marina Evgenievna, Shundrina I. K. Inna Kazimirovna, Zaytseva E. V. Elena Vasiljevna, Parkhomenko D. A. Dmitry Aleksandrovich, Bagryanskaya E. G. Elena Grigorjevna, Ovcharenko V. I. Viktor Ivanovich
Riassunto:Title screen
Thermally stable organic diradicals with a triplet ground state along with large singlet-triplet energy gap have significant potential for advanced technological applications. A series of phenylene-bridged diradicals with oxoverdazyl and nitronyl nitroxide units were synthesized via a palladium-catalyzed cross-coupling reaction of iodoverdazyls with a nitronyl nitroxide-2-ide gold(I) complex with high yields. The diradicals exhibit high stability and do not decompose in an inert atmosphere up to 180?°C. For the diradicals, both substantial AF (?EST˜-64 cm-1) and FM (?EST=25 and 100 cm-1) intramolecular exchange interactions were observed. The sign of the exchange interaction is determined both by the bridging moiety (para- or meta-phenylene) and by the type of oxoverdazyl block (C-linked or N-linked). Upon crystallization, diradicals with the triplet ground state form unique one-dimensional exchange-coupled chains with strong intra- and weak inter-diradical ferromagnetic coupling.
Режим доступа: по договору с организацией-держателем ресурса
Lingua:inglese
Pubblicazione: 2020
Soggetti:
Accesso online:https://doi.org/10.1002/anie.202010041
Natura: MixedMaterials Elettronico Capitolo di libro
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=663336

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200 1 |a Ferromagnetically Coupled S=1 Chains in Crystals of Verdazyl-Nitronyl Nitroxide Diradicals  |f E. V. Tretjyakov, S. I. Zhivetjeva, P. V. Petunin [et al.] 
203 |a Text  |c electronic 
300 |a Title screen 
320 |a [References: 9 tit.] 
330 |a Thermally stable organic diradicals with a triplet ground state along with large singlet-triplet energy gap have significant potential for advanced technological applications. A series of phenylene-bridged diradicals with oxoverdazyl and nitronyl nitroxide units were synthesized via a palladium-catalyzed cross-coupling reaction of iodoverdazyls with a nitronyl nitroxide-2-ide gold(I) complex with high yields. The diradicals exhibit high stability and do not decompose in an inert atmosphere up to 180?°C. For the diradicals, both substantial AF (?EST˜-64 cm-1) and FM (?EST=25 and 100 cm-1) intramolecular exchange interactions were observed. The sign of the exchange interaction is determined both by the bridging moiety (para- or meta-phenylene) and by the type of oxoverdazyl block (C-linked or N-linked). Upon crystallization, diradicals with the triplet ground state form unique one-dimensional exchange-coupled chains with strong intra- and weak inter-diradical ferromagnetic coupling. 
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463 |t Vol. 59, iss. 46  |v [P. 20704-20710]  |d 2020 
610 1 |a электронный ресурс 
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610 1 |a BS-DFT and high level calculations 
610 1 |a ferromagnetic chain 
610 1 |a high-spin molecules 
610 1 |a nitroxides 
610 1 |a triplet diradicals 
610 1 |a ферромагнитные цепи 
701 1 |a Tretjyakov  |b E. V.  |g Evgeny Viktorovich 
701 1 |a Zhivetjeva  |b S. I.  |g Svetlana Ivanovna 
701 1 |a Petunin  |b P. V.  |c chemist  |c Associate Professor of Tomsk Polytechnic University, Candidate of Chemical Sciences  |f 1982-  |g Pavel Vasilievich  |3 (RuTPU)RU\TPU\pers\36904  |9 19933 
701 1 |a Gorbunov  |b D. E.  |g Dmitry Evgenjevich 
701 1 |a Gritsan  |b N. P.  |g Nina Petrovna 
701 1 |a Bagryanskaya  |b I. Yu.  |g Irina Yurjevna 
701 1 |a Bogomyakov  |b A. S.  |g Artem Stepanovich 
701 1 |a Postnikov  |b P. S.  |c organic chemist  |c Associate Professor of Tomsk Polytechnic University, Candidate of chemical sciences  |f 1984-  |g Pavel Sergeevich  |3 (RuTPU)RU\TPU\pers\31287  |9 15465 
701 1 |a Kazantsev  |b M. S.  |g Maksim Sergeevich 
701 1 |a Trusova  |b M. E.  |c organic chemist  |c Associate professor of Tomsk Polytechnic University, Candidate of chemical sciences  |f 1982-  |g Marina Evgenievna  |3 (RuTPU)RU\TPU\pers\31823  |9 15918 
701 1 |a Shundrina  |b I. K.  |g Inna Kazimirovna 
701 1 |a Zaytseva  |b E. V.  |g Elena Vasiljevna 
701 1 |a Parkhomenko  |b D. A.  |g Dmitry Aleksandrovich 
701 1 |a Bagryanskaya  |b E. G.  |g Elena Grigorjevna 
701 1 |a Ovcharenko  |b V. I.  |g Viktor Ivanovich 
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