Influence of preceramic paper composition on microstructure and mechanical properties of spark plasma sintered Ti3SiC2-based composites; Journal of Physics: Conference Series; Vol. 1611 : Prospects of Fundamental Sciences Development (PFSD-2020)

Dades bibliogràfiques
Parent link:Journal of Physics: Conference Series
Vol. 1611 : Prospects of Fundamental Sciences Development (PFSD-2020).— 2020.— [012007, 6 p.]
Autor corporatiu: Национальный исследовательский Томский политехнический университет Инженерная школа ядерных технологий Отделение экспериментальной физики, Национальный исследовательский Томский политехнический университет Инженерная школа ядерных технологий Отделение ядерно-топливного цикла, Национальный исследовательский Томский политехнический университет Инженерная школа новых производственных технологий Отделение материаловедения
Altres autors: Sedanova E. P. Elizaveta Pavlovna, Kashkarov E. B. Egor Borisovich, Syrtanov M. S. Maksim Sergeevich, Abdullina K. R. Kristina Rinatovna, Mingazova Yu. R. Yuliya Rafailovna, Lider A. M. Andrey Markovich, Travitsky (Travitzky) N. Nakhum
Sumari:Title screen
This paper describes the effect of preceramic paper composition on microstructure and mechanical properties of Ti3SiC2-based composites. The preceramic paper with Ti3SiC2-powder filler and different content (from 10 to 40 wt.%) of organic component (cellulose) was prepared. The composites were obtained by spark plasma sintering (SPS) at 50 MPa pressure for 10 min holding time. The sintering temperature was 1473 K. The influence of organic content on microstructure, phase composition, and flexural strength of the sintered materials was analyzed by scanning electron microscopy (SEM), X-ray diffraction (XRD) and mechanical testing, respectively. It was revealed that the microstructure of the sintered materials became more porous with increasing of cellulose content in the paper. XRD analysis showed the presence of Ti3SiC2, TiC and TiSi2 phases in the sintered samples while the content of the Ti3SiC2 phase increase with decreasing of the organic content. The flexural strength changes from 100 (40 wt.%) to 300 MPa (10 wt.% organic binder) that is caused by porosity of the composites.
Idioma:anglès
Publicat: 2020
Matèries:
Accés en línia:https://doi.org/10.1088/1742-6596/1611/1/012007
http://earchive.tpu.ru/handle/11683/63233
Format: MixedMaterials Electrònic Capítol de llibre
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=662664

MARC

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200 1 |a Influence of preceramic paper composition on microstructure and mechanical properties of spark plasma sintered Ti3SiC2-based composites  |f E. P. Sedanova, E. B. Kashkarov, M. S. Syrtanov [et al.] 
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330 |a This paper describes the effect of preceramic paper composition on microstructure and mechanical properties of Ti3SiC2-based composites. The preceramic paper with Ti3SiC2-powder filler and different content (from 10 to 40 wt.%) of organic component (cellulose) was prepared. The composites were obtained by spark plasma sintering (SPS) at 50 MPa pressure for 10 min holding time. The sintering temperature was 1473 K. The influence of organic content on microstructure, phase composition, and flexural strength of the sintered materials was analyzed by scanning electron microscopy (SEM), X-ray diffraction (XRD) and mechanical testing, respectively. It was revealed that the microstructure of the sintered materials became more porous with increasing of cellulose content in the paper. XRD analysis showed the presence of Ti3SiC2, TiC and TiSi2 phases in the sintered samples while the content of the Ti3SiC2 phase increase with decreasing of the organic content. The flexural strength changes from 100 (40 wt.%) to 300 MPa (10 wt.% organic binder) that is caused by porosity of the composites. 
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701 1 |a Kashkarov  |b E. B.  |c Physicist  |c Associate Professor, Researcher of Tomsk Polytechnic University, Candidate of Physical and Mathematical Sciences  |f 1991-  |g Egor Borisovich  |3 (RuTPU)RU\TPU\pers\34949  |9 18267 
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