Fabrication of Paper-Derived Ti3SiC2-Based Materials by Spark Plasma Sintering; Advanced Engineering Materials; Vol. 22, iss. 6
| Parent link: | Advanced Engineering Materials Vol. 22, iss. 6.— 2020.— [2000136, 8 p.] |
|---|---|
| সংস্থা লেখক: | , , |
| অন্যান্য লেখক: | , , , , , |
| সংক্ষিপ্ত: | Title screen Novel paper-derived Ti3SiC2-based ceramics are fabricated by spark plasma sintering (SPS). A Ti3SiC2-loaded preceramic article is used as feedstock. The sintering temperature and pressure are 1100–1200?°C and 20–50?MPa, respectively. The influence of sintering parameters on phase composition and microstructure is analyzed by X-ray diffraction (XRD) and scanning electron microscopy, respectively. In addition, energy-dispersive X-ray spectroscopy is conducted to analyze the distribution of elements and the phase arrangement depending on the sintering temperature. XRD analysis of the composites sintered at 1100 and 1200?°C shows the presence of Ti3SiC2, TiC, and TiSi2 phases while the content of Ti3SiC2 phase decreases with increasing temperature. It is shown that an increase in both temperature and pressure lead to higher densification of the composites. Elongated pores are observed in the composites, which are formed as a result of cellulose fiber decomposition during the sintering process. The maximal value of the flexural strength of 300?MPa is measured for the composite with the highest density. The influence of SPS parameters on the formation of phase composition, microstructure, and mechanical properties of the paper-derived Ti3SiC2-based ceramics is discussed. |
| ভাষা: | ইংরেজি |
| প্রকাশিত: |
2020
|
| বিষয়গুলি: | |
| অনলাইন ব্যবহার করুন: | https://doi.org/10.1002/adem.202000136 |
| বিন্যাস: | বৈদ্যুতিক গ্রন্থের অধ্যায় |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=662602 |
MARC
| LEADER | 00000naa0a2200000 4500 | ||
|---|---|---|---|
| 001 | 662602 | ||
| 005 | 20250712062929.0 | ||
| 035 | |a (RuTPU)RU\TPU\network\33757 | ||
| 090 | |a 662602 | ||
| 100 | |a 20200909d2020 k||y0rusy50 ba | ||
| 101 | 0 | |a eng | |
| 102 | |a US | ||
| 135 | |a drcn ---uucaa | ||
| 181 | 0 | |a i | |
| 182 | 0 | |a b | |
| 200 | 1 | |a Fabrication of Paper-Derived Ti3SiC2-Based Materials by Spark Plasma Sintering |f E. B. Kashkarov, M. S. Syrtanov, E. P. Sedanova [et al.] | |
| 203 | |a Text |c electronic | ||
| 300 | |a Title screen | ||
| 320 | |a [References: 48 tit.] | ||
| 330 | |a Novel paper-derived Ti3SiC2-based ceramics are fabricated by spark plasma sintering (SPS). A Ti3SiC2-loaded preceramic article is used as feedstock. The sintering temperature and pressure are 1100–1200?°C and 20–50?MPa, respectively. The influence of sintering parameters on phase composition and microstructure is analyzed by X-ray diffraction (XRD) and scanning electron microscopy, respectively. In addition, energy-dispersive X-ray spectroscopy is conducted to analyze the distribution of elements and the phase arrangement depending on the sintering temperature. XRD analysis of the composites sintered at 1100 and 1200?°C shows the presence of Ti3SiC2, TiC, and TiSi2 phases while the content of Ti3SiC2 phase decreases with increasing temperature. It is shown that an increase in both temperature and pressure lead to higher densification of the composites. Elongated pores are observed in the composites, which are formed as a result of cellulose fiber decomposition during the sintering process. The maximal value of the flexural strength of 300?MPa is measured for the composite with the highest density. The influence of SPS parameters on the formation of phase composition, microstructure, and mechanical properties of the paper-derived Ti3SiC2-based ceramics is discussed. | ||
| 461 | |t Advanced Engineering Materials | ||
| 463 | |t Vol. 22, iss. 6 |v [2000136, 8 p.] |d 2020 | ||
| 610 | 1 | |a электронный ресурс | |
| 610 | 1 | |a труды учёных ТПУ | |
| 610 | 1 | |a microstructures | |
| 610 | 1 | |a paper-derived ceramics | |
| 610 | 1 | |a phase compositions | |
| 610 | 1 | |a preceramic papers | |
| 610 | 1 | |a spark plasma sintering | |
| 610 | 1 | |a микроструктуры | |
| 610 | 1 | |a керамика | |
| 610 | 1 | |a фазовые составы | |
| 610 | 1 | |a плазменное спекание | |
| 701 | 1 | |a Kashkarov |b E. B. |c Physicist |c Associate Professor, Researcher of Tomsk Polytechnic University, Candidate of Physical and Mathematical Sciences |f 1991- |g Egor Borisovich |3 (RuTPU)RU\TPU\pers\34949 |9 18267 | |
| 701 | 1 | |a Syrtanov |b M. S. |c physicist |c Associate Professor, Researcher of Tomsk Polytechnic University, Candidate of Technical Sciences |f 1990- |g Maksim Sergeevich |3 (RuTPU)RU\TPU\pers\34764 |9 18114 | |
| 701 | 1 | |a Sedanova |b E. P. |c Specialist in the field of nuclear technologies |c Engineer of Tomsk Polytechnic University |f 1994- |g Elizaveta Pavlovna |3 (RuTPU)RU\TPU\pers\45399 |9 21923 | |
| 701 | 1 | |a Ivashutenko |b A. S. |c specialist in the field of electrical engineering |c Associate Professor of the Tomsk Polytechnic University, Candidate of technical sciences |f 1981- |g Alexander Sergeevich |3 (RuTPU)RU\TPU\pers\33076 |9 16908 | |
| 701 | 1 | |a Lider |b A. M. |c Physicist |c Professor of Tomsk Polytechnic University, Doctor of Technical Sciences |f 1976-2025 |g Andrey Markovich |y Tomsk |3 (RuTPU)RU\TPU\pers\30400 |9 14743 | |
| 701 | 1 | |a Travitsky (Travitzky) |b N. |c specialist in the field of material science |c Professor of Tomsk Polytechnic University |f 1951- |g Nakhum |3 (RuTPU)RU\TPU\pers\42461 |9 21540 | |
| 712 | 0 | 2 | |a Национальный исследовательский Томский политехнический университет |b Инженерная школа ядерных технологий |b Отделение экспериментальной физики |3 (RuTPU)RU\TPU\col\23549 |9 28346 |
| 712 | 0 | 2 | |a Национальный исследовательский Томский политехнический университет |b Инженерная школа энергетики |b Отделение электроэнергетики и электротехники (ОЭЭ) |3 (RuTPU)RU\TPU\col\23505 |
| 712 | 0 | 2 | |a Национальный исследовательский Томский политехнический университет |b Инженерная школа новых производственных технологий |b Отделение материаловедения |3 (RuTPU)RU\TPU\col\23508 |9 28324 |
| 801 | 2 | |a RU |b 63413507 |c 20200909 |g RCR | |
| 856 | 4 | |u https://doi.org/10.1002/adem.202000136 | |
| 942 | |c CF | ||