The Hydrothermal Synthesis Duration Influence on Calcium Phosphate and Hydroxyapatite Phase Composition; IOP Conference Series: Materials Science and Engineering; Vol. 731 : Advanced Materials for Engineering and Medicine (AMEM-2019)
| Parent link: | IOP Conference Series: Materials Science and Engineering Vol. 731 : Advanced Materials for Engineering and Medicine (AMEM-2019).— 2020.— [012024, 7 p.] |
|---|---|
| Autor kompanije: | |
| Daljnji autori: | , , , , , , |
| Sažetak: | Title screen This paper reports the hydrothermal synthesis process duration influence on phase composition, crystallinity degree, morphology and dispersity of the hydroxyapatite powder. The calcium phosphate and hydroxyapatite were synthesized in precursor system Ca(NO[3])[2](NH[4])[2]HPO[4]-NH[4]OH. The obtained powders were characterized with X-Ray diffraction, Fourier Transform spectroscopy (FTIR) and Raman spectroscopy. The results demonstrate: the increasing of the synthesis time duration has no influence on the phase composition. However, the synthesis duration time growth from 12 to 48 hours make possible increase the crystallinity degree from 0.68 to 0.98. |
| Jezik: | engleski |
| Izdano: |
2020
|
| Teme: | |
| Online pristup: | http://dx.doi.org/10.1088/1757-899X/731/1/012024 http://earchive.tpu.ru/handle/11683/58051 |
| Format: | Elektronički Poglavlje knjige |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=661951 |
| Sažetak: | Title screen This paper reports the hydrothermal synthesis process duration influence on phase composition, crystallinity degree, morphology and dispersity of the hydroxyapatite powder. The calcium phosphate and hydroxyapatite were synthesized in precursor system Ca(NO[3])[2](NH[4])[2]HPO[4]-NH[4]OH. The obtained powders were characterized with X-Ray diffraction, Fourier Transform spectroscopy (FTIR) and Raman spectroscopy. The results demonstrate: the increasing of the synthesis time duration has no influence on the phase composition. However, the synthesis duration time growth from 12 to 48 hours make possible increase the crystallinity degree from 0.68 to 0.98. |
|---|---|
| Digitalni identifikator objekta: | 10.1088/1757-899X/731/1/012024 |