Synthesis and antioxidant activity of some new thioglycoluril derivatives; Journal of Sulfur Chemistry; Vol. 32, iss. 1
| Parent link: | Journal of Sulfur Chemistry Vol. 32, iss. 1.— 2019.— [P. 3-16] |
|---|---|
| Corporate Authors: | , |
| Other Authors: | , , , , |
| Summary: | Title screen A series of S-alkylated products was prepared by alkylation of thioglycoluril with various alkylation agents, i.e. ethyl bromide, ethylene dibromide and chloroacetic acid. The synthesis performed in DMF at 60°C using sodium hydroxide as a base to give the corresponding products with significant advantages such as high conversions, short reaction time, mild reaction conditions, and low cost, simple workup with moderate to excellent yields. The structures of the synthesized compounds have been deduced from their spectral (IR, 1H-NMR and 13C-NMR) data. Significant antioxidant activity was observed for some members of the series. Режим доступа: по договору с организацией-держателем ресурса |
| Language: | English |
| Published: |
2019
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| Subjects: | |
| Online Access: | https://doi.org/10.1080/17415993.2019.1588897 |
| Format: | Electronic Book Chapter |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=661347 |
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| 200 | 1 | |a Synthesis and antioxidant activity of some new thioglycoluril derivatives |f I. Boudebouz [et al.] | |
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| 300 | |a Title screen | ||
| 320 | |a [References: 31 tit.] | ||
| 330 | |a A series of S-alkylated products was prepared by alkylation of thioglycoluril with various alkylation agents, i.e. ethyl bromide, ethylene dibromide and chloroacetic acid. The synthesis performed in DMF at 60°C using sodium hydroxide as a base to give the corresponding products with significant advantages such as high conversions, short reaction time, mild reaction conditions, and low cost, simple workup with moderate to excellent yields. The structures of the synthesized compounds have been deduced from their spectral (IR, 1H-NMR and 13C-NMR) data. Significant antioxidant activity was observed for some members of the series. | ||
| 333 | |a Режим доступа: по договору с организацией-держателем ресурса | ||
| 461 | |t Journal of Sulfur Chemistry | ||
| 463 | |t Vol. 32, iss. 1 |v [P. 3-16] |d 2019 | ||
| 610 | 1 | |a электронный ресурс | |
| 610 | 1 | |a труды учёных ТПУ | |
| 610 | 1 | |a thioglycoluril | |
| 610 | 1 | |a alkylation | |
| 610 | 1 | |a alkyl halides | |
| 610 | 1 | |a hioamides | |
| 610 | 1 | |a antioxidant activity | |
| 610 | 1 | |a алкилирование | |
| 610 | 1 | |a алкилгалогениды | |
| 610 | 1 | |a антиоксидантная активность | |
| 701 | 1 | |a Boudebouz |b I. |g Imene | |
| 701 | 1 | |a Arrous |b S. |g Salah | |
| 701 | 1 | |a Plotnikov |b E. V. |c chemist |c Engineer of Tomsk Polytechnic University |f 1983- |g Evgeny Vladimirovich |3 (RuTPU)RU\TPU\pers\32469 | |
| 701 | 1 | |a Voronova |b O. A. |c chemist |c Assistant of Tomsk Polytechnic University, Candidate of chemical sciences |f 1979- |g Olesya Aleksandrovna |3 (RuTPU)RU\TPU\pers\32169 |9 16170 | |
| 701 | 1 | |a Bakibaev |b A. A. |c Russian chemist |c Professor of TPU, doctor of chemical sciences |f 1960- |g Abdigali Abdimanapovich |3 (RuTPU)RU\TPU\pers\27851 | |
| 712 | 0 | 2 | |a Национальный исследовательский Томский политехнический университет |b Исследовательская школа химических и биомедицинских технологий |c (2017- ) |3 (RuTPU)RU\TPU\col\23537 |
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