Synthesis and antioxidant activity of some new thioglycoluril derivatives

Synthesis and antioxidant activity of some new thioglycoluril derivatives

Bibliografiske detaljer
Parent link:Journal of Sulfur Chemistry
Vol. 32, iss. 1.— 2019.— [P. 3-16]
Corporate Authors: Национальный исследовательский Томский политехнический университет Исследовательская школа химических и биомедицинских технологий, Национальный исследовательский Томский политехнический университет Инженерная школа природных ресурсов Отделение химической инженерии
Andre forfattere: Boudebouz I. Imene, Arrous S. Salah, Plotnikov E. V. Evgeny Vladimirovich, Voronova O. A. Olesya Aleksandrovna, Bakibaev A. A. Abdigali Abdimanapovich
Summary:Title screen
A series of S-alkylated products was prepared by alkylation of thioglycoluril with various alkylation agents, i.e. ethyl bromide, ethylene dibromide and chloroacetic acid. The synthesis performed in DMF at 60°C using sodium hydroxide as a base to give the corresponding products with significant advantages such as high conversions, short reaction time, mild reaction conditions, and low cost, simple workup with moderate to excellent yields. The structures of the synthesized compounds have been deduced from their spectral (IR, 1H-NMR and 13C-NMR) data. Significant antioxidant activity was observed for some members of the series.
Режим доступа: по договору с организацией-держателем ресурса
Udgivet: 2019
Fag:
электронный ресурс
труды учёных ТПУ
thioglycoluril
alkylation
alkyl halides
hioamides
antioxidant activity
алкилирование
алкилгалогениды
антиоксидантная активность
Online adgang:https://doi.org/10.1080/17415993.2019.1588897
Format: Electronisk Book Chapter
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=661347
Beskrivelse
Summary:Title screen
A series of S-alkylated products was prepared by alkylation of thioglycoluril with various alkylation agents, i.e. ethyl bromide, ethylene dibromide and chloroacetic acid. The synthesis performed in DMF at 60°C using sodium hydroxide as a base to give the corresponding products with significant advantages such as high conversions, short reaction time, mild reaction conditions, and low cost, simple workup with moderate to excellent yields. The structures of the synthesized compounds have been deduced from their spectral (IR, 1H-NMR and 13C-NMR) data. Significant antioxidant activity was observed for some members of the series.
Режим доступа: по договору с организацией-держателем ресурса
DOI:10.1080/17415993.2019.1588897

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