Effect of ball milling on defects level, Curie point and microstructure of LiTiZn ferrite ceramics; Journal of Thermal Analysis and Calorimetry; Vol. 138, iss. 3

Xehetasun bibliografikoak
Parent link:Journal of Thermal Analysis and Calorimetry
Vol. 138, iss. 3.— 2019.— [P. 2197-2203]
Egile korporatiboa: Национальный исследовательский Томский политехнический университет Институт неразрушающего контроля Проблемная научно-исследовательская лаборатория электроники, диэлектриков и полупроводников, Национальный исследовательский Томский политехнический университет Инженерная школа неразрушающего контроля и безопасности Отделение контроля и диагностики
Beste egile batzuk: Malyshev A. V. Andrei Vladimirovich, Vlasov V. A. Vitaliy Anatolievich, Petrova A. B. Anna Borisovna, Surzhikov A. P. Anatoly Petrovich
Gaia:Title screen
In a present work, a comparative study of two types of LiTiZn samples of ferrite ceramics, which were sintered using conventional ceramic technology at a temperature of 1010 °C for 2 h and which were made with preliminary mechanical treatment in a ball planetary mill, was carried out. It is shown that mechanical treatment in a ball mill leads to a decrease in the defects level, an increase in the Curie point and a demagnetizing factor of ferrite ceramics. The growth of the demagnetizing factor is associated with an increase in the porosity of ferrite ceramics samples pre-grinded in ball. According to the X-ray phase analysis data, the lattice parameter and the coherent scattering region decrease in this case, and the microstrain is reduced by an order of magnitude. The defects level was assessed by the results of mathematical processing of the temperature dependences of the initial permeability using the previously proposed phenomenological expression. Measuring TG/DTG curves in a magnetic field allowed, on the one hand, to confirm a significant difference in Curie points for different types of samples, on the other hand, to detect the presence of an additional magnetic phase in ball-milled ferrite ceramics samples.
Режим доступа: по договору с организацией-держателем ресурса
Hizkuntza:ingelesa
Argitaratua: 2019
Gaiak:
Sarrera elektronikoa:https://doi.org/10.1007/s10973-019-08823-3
Formatua: Baliabide elektronikoa Liburu kapitulua
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=661203

MARC

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200 1 |a Effect of ball milling on defects level, Curie point and microstructure of LiTiZn ferrite ceramics  |f A. V. Malyshev [et al.] 
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330 |a In a present work, a comparative study of two types of LiTiZn samples of ferrite ceramics, which were sintered using conventional ceramic technology at a temperature of 1010 °C for 2 h and which were made with preliminary mechanical treatment in a ball planetary mill, was carried out. It is shown that mechanical treatment in a ball mill leads to a decrease in the defects level, an increase in the Curie point and a demagnetizing factor of ferrite ceramics. The growth of the demagnetizing factor is associated with an increase in the porosity of ferrite ceramics samples pre-grinded in ball. According to the X-ray phase analysis data, the lattice parameter and the coherent scattering region decrease in this case, and the microstrain is reduced by an order of magnitude. The defects level was assessed by the results of mathematical processing of the temperature dependences of the initial permeability using the previously proposed phenomenological expression. Measuring TG/DTG curves in a magnetic field allowed, on the one hand, to confirm a significant difference in Curie points for different types of samples, on the other hand, to detect the presence of an additional magnetic phase in ball-milled ferrite ceramics samples. 
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461 |t Journal of Thermal Analysis and Calorimetry 
463 |t Vol. 138, iss. 3  |v [P. 2197-2203]  |d 2019 
610 1 |a электронный ресурс 
610 1 |a труды учёных ТПУ 
610 1 |a ferrite ceramics 
610 1 |a ball milling 
610 1 |a sintering 
610 1 |a microstructure 
610 1 |a defects level 
610 1 |a magnetic properties 
610 1 |a ферритовая керамика 
610 1 |a фрезерование 
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701 1 |a Vlasov  |b V. A.  |c Physicist  |c Senior researcher of Tomsk Polytechnic University, Candidate of physical and mathematical sciences  |f 1975-  |g Vitaliy Anatolievich  |3 (RuTPU)RU\TPU\pers\31405  |9 15577 
701 1 |a Petrova  |b A. B.  |c specialist in the field of non-destructive testing  |c Associate Scientist of Tomsk Polytechnic University  |f 1992-  |g Anna Borisovna  |3 (RuTPU)RU\TPU\pers\36438 
701 1 |a Surzhikov  |b A. P.  |c physicist  |c Professor of Tomsk Polytechnic University, doctor of physical and mathematical sciences (DSc)  |f 1951-  |g Anatoly Petrovich  |3 (RuTPU)RU\TPU\pers\30237  |9 14617 
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