Thermal stability of Ti-45Nb mechanically alloyed powder; Письма о материалах; Т. 8, № 4 (32)

Bibliographic Details
Parent link:	Письма о материалах=Letters on Materials/ Российская академия наук (РАН), Институт проблем сверхпластичности металлов (ИПСМ) Т. 8, № 4 (32).— 2018.— [С. 443-447]
Corporate Authors:	Национальный исследовательский Томский политехнический университет Инженерная школа новых производственных технологий Отделение материаловедения, Национальный исследовательский Томский политехнический университет Исследовательская школа физики высокоэнергетических процессов
Other Authors:	Kovalevskaya Zh. G. Zhanna Gennadievna, Sharkeev Yu. P. Yury Petrovich, Khimich M. A. Margarita Andreevna, Glukhov I. A. Ivan Aleksandrovich
Summary:	Заглавие с экрана Текст на английском языке The thermal stability of Ti-45Nb powder obtained via mechanical alloying of pure components Ti and Nb using an AGO-2C high energy planetary ball mill was studied. To evaluate the structure and phase transformations in the material, scanning and transmission electron microscopic studies and x-ray diffraction analysis were carried out. Mechanical alloying of titanium and niobium powders occurs under the conditions of severe plastic deformation and leads to the homogenization of initial components. As a result, an alloy with the structure consisting of a mixture of different grains is formed. This mixture of nanosized grains consists of the main ?-TiNb phase and metastable ?- and ?"-phases. The presence of metastable phases, large amount of interfaces, lattice distortions of the main phase indicate the presence of high internal energy stored in the material. By means of differential scanning calorimetric analysis it was found that structural and phase transformations occurred during heating of the powder up to temperatures of about 500°C and 700°C. During annealing at 500°C the mechanically alloyed powder loses the metastable ?"-phase while the ?-phase becomes equilibrium. At the same time, the process of recrystallization nuclei formation starts in the structure. The annealing at 700°C does not change the phase composition of the alloy. The exothermal effect observed at this temperature is related to structural transformations in the alloy, in other words, to the recrystallization of plastically deformed material. Basing on the results obtained it was concluded, that the upper limit of the thermal stability of mechanically alloyed Ti-45Nb powder does not exceed 500°C. Режим доступа: по договору с организацией-держателем ресурса
Language:	English
Published:	2018
Subjects:	электронный ресурс труды учёных ТПУ механическое легирование мельницы порошки термостабильность отжиг
Online Access:	https://elibrary.ru/item.asp?id=36819853 https://doi.org/10.22226/2410-3535-2018-4-443-447
Format:	Electronic Book Chapter
KOHA link:	https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=660201