Quantitative and Qualitative Analysis of Hydrogen Accumulation in Hydrogen-Storage Materials Using Hydrogen Extraction in an Inert Atmosphere

Quantitative and Qualitative Analysis of Hydrogen Accumulation in Hydrogen-Storage Materials Using Hydrogen Extraction in an Inert Atmosphere

Detalles Bibliográficos
Parent link:Metals
Vol. 8, iss. 9.— 2018.— [672, 11 p.]
Autor Corporativo: Национальный исследовательский Томский политехнический университет Инженерная школа ядерных технологий Отделение экспериментальной физики
Otros Autores: Babikhina M. N. Mariya Nikolaevna, Kudiyarov V. N. Victor Nikolaevich, Mostovshchikov A. V. Andrey Vladimirovich, Lider A. M. Andrey Markovich
Sumario:Title screen
Currently, standard samples with high hydrogen concentrations that meet the requirements of hydrogen extraction in an inert atmosphere are not currently available on the market. This article describes the preparation of Ti-H standard samples and the calibration of RHEN602, a hydrogen analyzer, using LECO (LECO, Saint Joseph, MI, USA). Samples of technically pure titanium alloy were chosen as the material for sample production. The creation procedure includes five main steps: sample preparation (polishing to an average roughness of 0.04 ?m using sandpaper), annealing, hydrogenation, maintenance in an inert gas atmosphere, and characterization of the samples. The absolute hydrogen concentration in the samples was determined by two methods: volumetric and mass change after the introduction of hydrogen. Furthermore, in-situ X-ray diffraction, temperature programmed desorption (TPD) analysis, and thermogravimetric analysis were used during measurements to investigate the phase transitions in the samples. As a result of this work, a series of calibration samples were prepared in a concentration range up to 4 wt % hydrogen, optimal parameters for measuring high concentrations of hydrogen. The calibration line was obtained and the calibration error was 10%.
Lenguaje:inglés
Publicado: 2018
Materias:
электронный ресурс
труды учёных ТПУ
RHEN602 by LECO
hydrogen
standard samples
titanium alloy
водород
стандартные образцы
титановые сплавы
Acceso en línea:https://doi.org/10.3390/met8090672
Formato: Electrónico Capítulo de libro
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=660132

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