Hydrogen calibration of GD-spectrometer using Zr-1Nb alloy; Applied Surface Science; Vol. 432, Pt. B

Hydrogen calibration of GD-spectrometer using Zr-1Nb alloy; Applied Surface Science; Vol. 432, Pt. B

Bibliographic Details
Parent link:	Applied Surface Science Vol. 432, Pt. B.— 2018.— [P. 85-89]
Corporate Author:	Национальный исследовательский Томский политехнический университет (ТПУ) Физико-технический институт (ФТИ) Кафедра общей физики (ОФ)
Other Authors:	Mikhaylov (Mikhailov) A. A. Andrey Anatolievich, Pryamushko T. S. Tatiana Sergeevna, Babikhina (Babihina) M. N. Mariya Nikolaevna, Kudiyarov V. N. Victor Nikolaevich, Heller R. Rene, Laptev R. S. Roman Sergeevich, Lider A. M. Andrey Markovich
Summary:	Title screen To study the hydrogen distribution in Zr-1Nb alloy (Э110 alloy) GD-OES was applied in this work. Qualitative analysis needs the standard samples with hydrogen. However, the standard samples with high concentrations of hydrogen in the zirconium alloy which would meet the requirements of the shape, size are absent. In this work method of Zr + H calibration samples production was performed at the first time. Automated Complex Gas Reaction Controller was used for samples hydrogenation. To calculate the parameters of post-hydrogenation incubation of the samples in an inert gas atmosphere the diffusion equations were used. Absolute hydrogen concentrations in the samples were determined by melting in the inert gas atmosphere using RHEN602 analyzer (LECO Company). Hydrogen distribution was studied using nuclear reaction analysis (HZDR, Dresden, Germany). RF GD-OES was used for calibration. The depth of the craters was measured with the help of a Hommel-Etamic profilometer by Jenoptik, Germany. Режим доступа: по договору с организацией-держателем ресурса
Language:	English
Published:	2018
Subjects:	электронный ресурс труды учёных ТПУ hydrogen calibration разряды эмиссионная спектроскопия водород калибровка циркониевые сплавы
Online Access:	https://doi.org/10.1016/j.apsusc.2017.06.191
Format:	Electronic Book Chapter
KOHA link:	https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=657338

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