An efficient multigram-scale synthesis of 4-([omega]-chloroalkoxy)phenols; Russian Chemical Bulletin; Vol. 66, iss. 2
| Parent link: | Russian Chemical Bulletin: Scientific Journal Vol. 66, iss. 2.— 2017.— [P. 304–312] |
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| Institution som forfatter: | |
| Andre forfattere: | , , , , , , , |
| Summary: | Title screen Efficient multigram two-step syntheses of 4-(2-chloroethoxy)phenol and 4-(3-chloropropoxy)phenol in >70% yields starting from 4-hydroxybenzaldehyde and reagents with general formula Cl(CH2)nX (X = Cl, n = 2; X = OTs, n = 3) are proposed. 4-(2-Chloroethoxy)phenol can also be conveniently prepared from 4-methoxyphenol and 1,2-dichloroethane. The compounds thus obtained can be used in carbohydrate chemistry to synthesize glycosides bearing "universal" 4-(ω-chloroalkoxy)phenyl aglycons. Режим доступа: по договору с организацией-держателем ресурса |
| Sprog: | engelsk |
| Udgivet: |
2017
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| Fag: | |
| Online adgang: | https://doi.org/10.1007/s11172-017-1732-9 |
| Format: | Electronisk Bog |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=655757 |
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| 200 | 1 | |a An efficient multigram-scale synthesis of 4-([omega]-chloroalkoxy)phenols |f A. I. Zinin [et al.] | |
| 203 | |a Text |c electronic | ||
| 300 | |a Title screen | ||
| 320 | |a [References: p. 311-312 (44 tit.)] | ||
| 330 | |a Efficient multigram two-step syntheses of 4-(2-chloroethoxy)phenol and 4-(3-chloropropoxy)phenol in >70% yields starting from 4-hydroxybenzaldehyde and reagents with general formula Cl(CH2)nX (X = Cl, n = 2; X = OTs, n = 3) are proposed. 4-(2-Chloroethoxy)phenol can also be conveniently prepared from 4-methoxyphenol and 1,2-dichloroethane. The compounds thus obtained can be used in carbohydrate chemistry to synthesize glycosides bearing "universal" 4-(ω-chloroalkoxy)phenyl aglycons. | ||
| 333 | |a Режим доступа: по договору с организацией-держателем ресурса | ||
| 461 | |t Russian Chemical Bulletin |o Scientific Journal | ||
| 463 | |t Vol. 66, iss. 2 |v [P. 304–312] |d 2017 | ||
| 610 | 1 | |a электронный ресурс | |
| 610 | 1 | |a труды учёных ТПУ | |
| 610 | 1 | |a anomeric protective groups | |
| 610 | 1 | |a 4-(ω-chloroalkoxy)phenols | |
| 610 | 1 | |a phenols | |
| 610 | 1 | |a selective demethylation | |
| 610 | 1 | |a heterobifunctional building blocks | |
| 610 | 1 | |a защитные группы | |
| 610 | 1 | |a фенолы | |
| 610 | 1 | |a селективная деметилирование | |
| 610 | 1 | |a гетеробифункциональные строительные блоки | |
| 701 | 1 | |a Zinin |b A. I. |g Aleksandr Ivanovich | |
| 701 | 1 | |a Stepanova |b E. V. |c chemist |c engineer of Tomsk Polytechnic University |f 1978- |g Elena Vladimirovna |2 stltpush |3 (RuTPU)RU\TPU\pers\34245 | |
| 701 | 1 | |a Jost |b U . | |
| 701 | 1 | |a Kondakov |b N. N. |g Nikolay Nikolaevich | |
| 701 | 1 | |a Shpirt |b A. M. |g Anna Mikhaylovna | |
| 701 | 1 | |a Chizhov |b A. O. |g Aleksandr Olegovich | |
| 701 | 1 | |a Torgov |b V. I. |g Vladimir Igorevich | |
| 701 | 1 | |a Kononov |b L. O. |g Leonid Olegovich | |
| 712 | 0 | 2 | |a Национальный исследовательский Томский политехнический университет (ТПУ) |b Институт физики высоких технологий (ИФВТ) |b Кафедра биотехнологии и органической химии (БИОХ) |h 6810 |2 stltpush |3 (RuTPU)RU\TPU\col\18693 |
| 801 | 2 | |a RU |b 63413507 |c 20171005 |g RCR | |
| 856 | 4 | |u https://doi.org/10.1007/s11172-017-1732-9 | |
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