Application of Synchrotron Radiation for In Situ XRD Investigation of Zirconium Hydrides Formation at Gas-phase Hydrogenation

Bibliografski detalji
Parent link:Physics Procedia: Scientific Journal.— , 2008-
Vol. 84 : Synchrotron and Free electron laser Radiation: generation and application" (SFR-2016).— 2016.— [P. 342-348]
Autor kompanije: Национальный исследовательский Томский политехнический университет (ТПУ) Физико-технический институт (ФТИ) Кафедра общей физики (ОФ)
Daljnji autori: Syrtanov M. S. Maksim Sergeevich, Kudiyarov V. N. Victor Nikolaevich, Kashkarov E. B. Egor Borisovich, Shmakov A. N. Aleksandr Nikolaevich, Vinokurov Z. S. Zakhar Sergeevich, Babikhina (Babihina) M. N. Mariya Nikolaevna, Zolotarev K. V. Konstantina Vladimirovich
Sažetak:Title screen
The zirconium alloy (Zr1%Nb) samples with a micron-thick nickel layer were investigated for hydrogen sorption ability.Hydrogenation was carried out by gas phase method at temperatures of 350, 450 and 550 ° C. Hydrogen pressure in chamber was1 atm. Hydrogen sorption curves were obtained on the automated complex Gas Reaction Controller. In situ X-ray diffractionmeasurements of the process of hydrogen saturation of samples were carried out at the station "Precision diffractometry» atSiberian Synchrotron and Terahertz Radiation Center of the Budker Institute of Nuclear Physics. Hydrogen absorption rate byZr1%Nb alloy increases by order of magnitude with increasing temperature. The phase transitions significantly affect the rate ofhydrogen absorption at constant temperature. Measurements were performed using SR from the VEPP-3 storage ring.
Izdano: 2016
Teme:
Online pristup:https://doi.org/10.1016/j.phpro.2016.11.058
Format: Elektronički Poglavlje knjige
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=654875

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