Difficulties with the Determination of Mercury in Foodstuffs by Stripping Voltammetry; Journal of Analytical Chemistry; Vol. 59, iss. 5

Difficulties with the Determination of Mercury in Foodstuffs by Stripping Voltammetry; Journal of Analytical Chemistry; Vol. 59, iss. 5

Bibliographic Details
Parent link:Journal of Analytical Chemistry
Vol. 59, iss. 5.— 2004.— [P. 468–473]
Other Authors: Batalova V. N., Zakharova E. A. Elsa Arminana, Slepchenko G. B. Galina Borisovna, Malygina M. V.
Summary:Title screen
The main problems with the determination of mercury in foodstuffs by stripping voltammetry were analyzed. The conditions for obtaining the analytical signal from mercury(II) at a gold-graphite electrode and for reducing the effect of interfering substances were refined. A simplified procedure for the preparation of foodstuff samples by the chemical (HNO3 + H2O2) and photochemical oxidation of samples was proposed. The determination conditions were optimized by the fractional factorial design of the experiments. It was shown that a gas-discharge XeBr excilamp can be used as an alternative to a mercury quartz lamp in the sample preparation of foodstuffs. The conditions for reducing the blank experiment and its contribution to the results of determination were considered.
Режим доступа: по договору с организацией-держателем ресурса
Language:English
Published: 2004
Subjects:
труды учёных ТПУ
электронный ресурс
вольтамперометрия
пищевые продукты
ртуть
анализ
определение
Online Access:http://dx.doi.org/10.1023/B:JANC.0000026240.78768.80
Format: Electronic Book Chapter
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=654849

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