Synthesis, Crystal Structure and Thermal Stability of 1D Linear Silver(I) Coordination Polymers with 1,1,2,2-Tetra(pyrazol-1-yl)ethane; Crystals; Vol. 6, iss. 11

Synthesis, Crystal Structure and Thermal Stability of 1D Linear Silver(I) Coordination Polymers with 1,1,2,2-Tetra(pyrazol-1-yl)ethane; Crystals; Vol. 6, iss. 11

Sonraí bibleagrafaíochta
Parent link:	Crystals Vol. 6, iss. 11.— 2016.— [138, 12 p.]
Údar corparáideach:	Национальный исследовательский Томский политехнический университет (ТПУ) Институт физики высоких технологий (ИФВТ) Кафедра биотехнологии и органической химии (БИОХ)
Rannpháirtithe:	Semitut E. Yu. Evgeny Yurjevich, Komarov V. Yu. Vladislav Yurievich, Sukhikh T. S. Taisiya Sergeevna, Filatov E. Yu. Evgeny Yurjevich, Potapov A. S. Andrey Sergeevich
Achoimre:	Title screen Two new linear silver(I) nitrate coordination polymers with bitopic ligand 1,1,2,2-tetra(pyrazol-1-yl)ethane were synthesized. Synthesized compounds were characterized by IR spectroscopy, elemental analysis, powder X-ray diffraction and thermal analysis. Silver coordination polymers demonstrated a yellow emission near 500 nm upon excitation at 360 nm. Crystal structures of coordination polymers were determined and structural peculiarities are discussed. In both of the structures, silver ions are connected via bridging ligand molecules to form polymeric chains with a five-atomic environment. The coordination environment of the central atom corresponds to a distorted trigonal bipyramid with two N atoms of different ligands in apical positions. The Ag–N bond distances vary in a wide range of 2.31–2.62 Е, giving strongly distorted metallacycles. Thermolysis of coordination polymers in reductive atmosphere (H2/He) leads to the formation of silver nanoparticles with a narrow size distribution.
Teanga:	Béarla
Foilsithe / Cruthaithe:	2016
Ábhair:	труды учёных ТПУ электронный ресурс silver coordination polymer bitopic ligand pyrazole crystal structure thermal analysis luminescence silver nanoparticles серебро координационные полимеры лиганды пиразол кристаллические структуры термический анализ люминесценция наночастицы
Rochtain ar líne:	http://dx.doi.org/10.3390/cryst6110138
Formáid:	Leictreonach Caibidil leabhair
KOHA link:	https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=653302

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