Combustion synthesis and characterization of porous Ni-Al materials for metal-supported solid oxide fuel cells application
| Parent link: | Journal of Alloys and Compounds Vol. 697.— 2017.— [P. 114–123] |
|---|---|
| Autor Corporativo: | |
| Otros Autores: | , , , |
| Sumario: | Title screen Combustion synthesis (CS) in thermal explosion mode under conditions of controlled heat loss is used for synthesis of thin Ni-Al porous plates. In the present work, compacted Ni-Al elemental powder mixtures placed between heat-removing clamp plates are heated in a furnace at 25 K/min up to 1000 K under the uniaxial load up to 1.2 MPa with further heat treatment at the temperature of 1100 K. The effects of the Ni/Al mass ratio, reagent powders size, porosity and thickness of the reacting samples as well as conditions of heat-exchange during the CS on the reaction parameters have been studied. Based on the thermocouple measurements, the temperature and timing characteristics of the CS process have been calculated. The phase composition evolution during the process has been analyzed using X-ray diffraction and energy-dispersive X-ray spectroscopy. Special attention has been paid to the study of the following characteristics of synthesized materials: porosity parameters, gas permeability and mechanical properties. Due to the high strength of synthesized materials and formation of relatively homogenous structure with proper pores size and gas permeability, the synthesized porous Ni-Al plates can be considered as good supporting substrate for application in metal-supported solid oxide fuel cells. |
| Lenguaje: | inglés |
| Publicado: |
2017
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| Materias: | |
| Acceso en línea: | http://dx.doi.org/10.1016/j.jallcom.2016.11.350 |
| Formato: | Electrónico Capítulo de libro |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=653152 |
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| 200 | 1 | |a Combustion synthesis and characterization of porous Ni-Al materials for metal-supported solid oxide fuel cells application |f A. S. Maznoy [et al.] | |
| 203 | |a Text |c electronic | ||
| 300 | |a Title screen | ||
| 320 | |a [References: р. 132 (30 tit.)] | ||
| 330 | |a Combustion synthesis (CS) in thermal explosion mode under conditions of controlled heat loss is used for synthesis of thin Ni-Al porous plates. In the present work, compacted Ni-Al elemental powder mixtures placed between heat-removing clamp plates are heated in a furnace at 25 K/min up to 1000 K under the uniaxial load up to 1.2 MPa with further heat treatment at the temperature of 1100 K. The effects of the Ni/Al mass ratio, reagent powders size, porosity and thickness of the reacting samples as well as conditions of heat-exchange during the CS on the reaction parameters have been studied. Based on the thermocouple measurements, the temperature and timing characteristics of the CS process have been calculated. The phase composition evolution during the process has been analyzed using X-ray diffraction and energy-dispersive X-ray spectroscopy. Special attention has been paid to the study of the following characteristics of synthesized materials: porosity parameters, gas permeability and mechanical properties. Due to the high strength of synthesized materials and formation of relatively homogenous structure with proper pores size and gas permeability, the synthesized porous Ni-Al plates can be considered as good supporting substrate for application in metal-supported solid oxide fuel cells. | ||
| 461 | |t Journal of Alloys and Compounds | ||
| 463 | |t Vol. 697 |v [P. 114–123] |d 2017 | ||
| 610 | 1 | |a электронный ресурс | |
| 610 | 1 | |a труды учёных ТПУ | |
| 610 | 1 | |a Porous Ni-Al | |
| 610 | 1 | |a синтез сжиганием | |
| 610 | 1 | |a combustion synthesis | |
| 610 | 1 | |a MS-SOFC | |
| 610 | 1 | |a топливные элементы | |
| 701 | 1 | |a Maznoy |b A. S. |g Anatoly Sergeevich | |
| 701 | 1 | |a Kirdyashkin |b A. I. |g Aleksandr Ivanovich | |
| 701 | 1 | |a Kitler |b V. D. |g Vladimir Davydovich | |
| 701 | 1 | |a Soloviev |b A. A. |c specialist in the field of hydrogen energy |c Associate Professor of Tomsk Polytechnic University, Candidate of technical sciences |f 1977- |g Andrey Aleksandrovich |3 (RuTPU)RU\TPU\pers\30863 | |
| 712 | 0 | 2 | |a Национальный исследовательский Томский политехнический университет (ТПУ) |b Физико-технический институт (ФТИ) |b Кафедра экспериментальной физики (ЭФ) |3 (RuTPU)RU\TPU\col\21255 |
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| 856 | 4 | |u http://dx.doi.org/10.1016/j.jallcom.2016.11.350 | |
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