Textural Characteristics of Products Obtained by Electrochemical Oxidation of Copper and Cadmium Using Alternating Current; Key Engineering Materials; Vol. 712 : Advanced Materials for Technical and Medical Purpose (AMTMP 2016)

Dades bibliogràfiques
Parent link:Key Engineering Materials: Scientific Journal
Vol. 712 : Advanced Materials for Technical and Medical Purpose (AMTMP 2016).— 2016.— [P. 112-116]
Autor corporatiu: Национальный исследовательский Томский политехнический университет (ТПУ) Институт физики высоких технологий (ИФВТ) Кафедра общей химии и химической технологии (ОХХТ), Национальный исследовательский Томский политехнический университет (ТПУ) Институт физики высоких технологий (ИФВТ) Кафедра технологии силикатов и наноматериалов (ТСН)
Altres autors: Dolinina A. S. Alesya Sergeevna, Korobochkin V. V. Valery Vasilievich, Usoltseva N. V. Natalia Vasilievna, Sudarev E. A. Evgeniy Aleksandrovich, Bikbaeva A. V. Alena, Popov M. V. Maxim
Sumari:Title screen
The porous structures of nanoparticles of copper and cadmium prepared by AC electrochemical synthesis in solutions of acetate of sodium, chlorides of ammonium and sodium were studied. It is established that at current density of 1A/cm{2} and concentration of NaCl 3 % wt. with the highest specific surface area (8.23m{2}/g), maximum pore volume (0.029 cm{3}/g) are formed, and the largest volume of the particles is characteristic of the nominal pore diameter - 62 nm. The values of specific surface area and total pore volume with increase in the temperature of calcination decrease, and the pores are slightly enlarged in diameter. Thus, the obtained data allow predicting operating parameters of the electrolysis to obtain copper - cadmium oxide system a predetermined porous structure.
Режим доступа: по договору с организацией-держателем ресурса
Idioma:anglès
Publicat: 2016
Col·lecció:Electrophysical and Electrochemical Methods and Technologies of Materials Treatment
Matèries:
Accés en línia:http://dx.doi.org/10.4028/www.scientific.net/KEM.712.112
Format: Electrònic Capítol de llibre
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=651269

MARC

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200 1 |a Textural Characteristics of Products Obtained by Electrochemical Oxidation of Copper and Cadmium Using Alternating Current  |f A. S. Dolinina [et al.] 
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330 |a The porous structures of nanoparticles of copper and cadmium prepared by AC electrochemical synthesis in solutions of acetate of sodium, chlorides of ammonium and sodium were studied. It is established that at current density of 1A/cm{2} and concentration of NaCl 3 % wt. with the highest specific surface area (8.23m{2}/g), maximum pore volume (0.029 cm{3}/g) are formed, and the largest volume of the particles is characteristic of the nominal pore diameter - 62 nm. The values of specific surface area and total pore volume with increase in the temperature of calcination decrease, and the pores are slightly enlarged in diameter. Thus, the obtained data allow predicting operating parameters of the electrolysis to obtain copper - cadmium oxide system a predetermined porous structure. 
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