Efficient one-stage procedure of Beckmann ketones rearrangement in the presence of hydroxylamine; Russian Journal of Organic Chemistry; Vol. 52, iss. 2

Efficient one-stage procedure of Beckmann ketones rearrangement in the presence of hydroxylamine; Russian Journal of Organic Chemistry; Vol. 52, iss. 2

Bibliografiske detaljer
Parent link:	Russian Journal of Organic Chemistry.— , 2001- Vol. 52, iss. 2.— 2016.— [P. 196-199]
Institution som forfatter:	Национальный исследовательский Томский политехнический университет Институт физики высоких технологий Кафедра биотехнологии и органической химии
Andre forfattere:	Kuksenok V. Yu. Vera Yurievna, Shtrykova V. V. Viktoriya Viktorovna, Filimonov V. D. Viktor Dmitrievich, Sidel’nikova S. P.
Summary:	Title screen Ketoximes formed from ketones in the presence of hydroxylamine and silica gel in formic acid undergo in situ the Beckmann rearrangement under mild conditions affording in high yields the corresponding amides. Unsymmetrical aromatic ketones, methyl aryl ketones, and methyl cyclohexyl ketone under these conditions form as a rule amides mixtures. Кетоксимы, образующиеся из кетонов в присутствии гидроксиламина и силикагеля в муравьиной кислоте, перегруппировываются in situ по Бекману в мягких условиях, образуя с высокими выходами соответствующие амиды. Несимметричные ароматические кетоны, метиларилкетоны и метилциклогексилкетон образуют в данных условиях, как правило, смеси амидов. Режим доступа: по договору с организацией-держателем ресурса
Sprog:	engelsk
Udgivet:	2016
Fag:	электронный ресурс труды учёных ТПУ
Online adgang:	http://dx.doi.org/10.1134/S1070428016020056
Format:	Electronisk Book Chapter
KOHA link:	https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=647662

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