Influence of Anodization Time and Voltage on the Parameters of TiO[2] Nanotubes; IOP Conference Series: Materials Science and Engineering; Vol. 116 : Advanced Materials and New Technologies in Modern Materials Science

Detalhes bibliográficos
Parent link:IOP Conference Series: Materials Science and Engineering
Vol. 116 : Advanced Materials and New Technologies in Modern Materials Science.— 2016.— [012025, 6 p.]
Autor principal: Chernozem R. V. Roman Viktorovich
Autor Corporativo: Национальный исследовательский Томский политехнический университет (ТПУ) Физико-технический институт (ФТИ) Кафедра теоретической и экспериментальной физики (ТиЭФ) Центр технологий (ЦТ)
Outros Autores: Surmeneva M. A. Maria Alexandrovna, Surmenev R. A. Roman Anatolievich
Resumo:Title screen
A vertically aligned titania nanotube layer was obtained by electrochemical anodic oxidation in the electrolyte contained 0.4 wt% solution of NH[4]F in 54 ml of ethylene glycol and 5 ml of deionized water, after titanium was chemically cleaned/etched with a mixture of HCl, H[2]O and HNO[3] solution for removing the natural oxide films. The morphology and composition of the titania nanotube layer were examined by scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS). The anodization of TiO[2] nanotubes was done using 60 V for 240 min and 30 min, and 30 V for 30 min. The diameter of the titania nanotubes was about 52-156 nm, the wall thickness about 32-53 nm and the height about 0.9-6.3 [mu]m. The pore size of TiO[2] nanotubes influences the dissolution rate of CaP thin films and Young's modulus, which is significantly lower than that of the Ti substrate. Our future challenge will be investigation of the microstructure and mechanical behavior of titania nanotubes with CaP film.
Режим доступа: по договору с организацией-держателем ресурса
Idioma:inglês
Publicado em: 2016
Assuntos:
Acesso em linha:http://dx.doi.org/10.1088/1757-899X/116/1/012025
http://earchive.tpu.ru/handle/11683/18926
Formato: Recurso Eletrônico Capítulo de Livro
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=647106

MARC

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200 1 |a Influence of Anodization Time and Voltage on the Parameters of TiO[2] Nanotubes  |f R. V. Chernozem, M. A. Surmeneva, R. A. Surmenev 
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330 |a A vertically aligned titania nanotube layer was obtained by electrochemical anodic oxidation in the electrolyte contained 0.4 wt% solution of NH[4]F in 54 ml of ethylene glycol and 5 ml of deionized water, after titanium was chemically cleaned/etched with a mixture of HCl, H[2]O and HNO[3] solution for removing the natural oxide films. The morphology and composition of the titania nanotube layer were examined by scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS). The anodization of TiO[2] nanotubes was done using 60 V for 240 min and 30 min, and 30 V for 30 min. The diameter of the titania nanotubes was about 52-156 nm, the wall thickness about 32-53 nm and the height about 0.9-6.3 [mu]m. The pore size of TiO[2] nanotubes influences the dissolution rate of CaP thin films and Young's modulus, which is significantly lower than that of the Ti substrate. Our future challenge will be investigation of the microstructure and mechanical behavior of titania nanotubes with CaP film. 
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