Investigation of Hydrogen Sorption-Desorption Processes and Hydrides Formation and Dissolution in Zirconium by Using Sievert Apparatus and Short-Wave Diffraction of Synchrotron Radiation

Bibliographic Details
Parent link:Key Engineering Materials: Scientific Journal
Vol. 683 : Multifunctional Materials: Development and Application.— 2016.— [P. 415-418]
Corporate Authors: Национальный исследовательский Томский политехнический университет (ТПУ) Физико-технический институт (ФТИ) Кафедра общей физики (ОФ), Национальный исследовательский Томский политехнический университет (ТПУ) Энергетический институт (ЭНИН) Кафедра атомных и тепловых электростанций (АТЭС)
Other Authors: Kudiyarov V. N. Victor Nikolaevich, Syrtanov M. S. Maksim Sergeevich, Babihina M. N., Gvozdyakov D. V. Dmitry Vasilievich
Summary:Title screen
Hydrogen sorption-desorption processes by zirconium alloy Zr-1Nb was investigated in this article. Sievert apparatus was used for investigation of hydrogen interaction with material. It was shown that hydrogenation at gas atmosphere at 350, 450 and 550 °С temperatures leads to the [delta]-hydride formation in all material volume. Hydrogen sorption rates were calculated on the linear parts of sorption curves and equal to 0.5·10{-4} wt%/s at 350 °С, 9.5·10{-4} wt%/s at 450 °С and 23.1·10{-4} wt%/s at 550 °С. Short-wave diffraction of synchrotron radiation was used for investigation of hydrides dissociation during heating. Hydrides dissociation formed after hydrogenation at gas atmosphere occurs at temperature 522-540 °С. Further temperature increasing leads to [beta]-phase appearance which indicates α to beta phase transition at zirconium.
Режим доступа: по договору с организацией-держателем ресурса
Language:English
Published: 2016
Series:Physicochemical Properties of Materials and Current Processing Technologies
Subjects:
Online Access:http://dx.doi.org/10.4028/www.scientific.net/KEM.683.415
Format: Electronic Book Chapter
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=646639

MARC

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200 1 |a Investigation of Hydrogen Sorption-Desorption Processes and Hydrides Formation and Dissolution in Zirconium by Using Sievert Apparatus and Short-Wave Diffraction of Synchrotron Radiation   |f V. N. Kudiyarov [et al.] 
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300 |a Title screen 
330 |a Hydrogen sorption-desorption processes by zirconium alloy Zr-1Nb was investigated in this article. Sievert apparatus was used for investigation of hydrogen interaction with material. It was shown that hydrogenation at gas atmosphere at 350, 450 and 550 °С temperatures leads to the [delta]-hydride formation in all material volume. Hydrogen sorption rates were calculated on the linear parts of sorption curves and equal to 0.5·10{-4} wt%/s at 350 °С, 9.5·10{-4} wt%/s at 450 °С and 23.1·10{-4} wt%/s at 550 °С. Short-wave diffraction of synchrotron radiation was used for investigation of hydrides dissociation during heating. Hydrides dissociation formed after hydrogenation at gas atmosphere occurs at temperature 522-540 °С. Further temperature increasing leads to [beta]-phase appearance which indicates α to beta phase transition at zirconium. 
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